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A novel method of prediction and optimization for preparative high-performance liquid chromatography separation
Jin, Yu1; Xue, Xingya1; Liu, Yanfang1; Xiao, Yuansheng1; Zhang, Jing1; Shi, Hui2; Zhang, Feifang1; Liang, Xinmiao1,2; Liang XM(梁鑫淼); Liang XM(梁鑫淼)
关键词Prediction Optimization Preparative High-performance Liquid Chromatography (Preparative Hplc) Retention Equation Complex Sample Traditional Chinese Medicine (Tcm)
刊名JOURNAL OF CHROMATOGRAPHY A
2008-03-07
DOI10.1016/j.chroma.2008.01.008
1183期:1-2页:76-86
收录类别SCI
文章类型Article
部门归属18
项目归属1803
产权排名1;1
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]GRADIENT ELUTION ; RETENTION TIMES ; PURIFICATION ; MODEL
英文摘要The preparation of components from a complex sample is a difficult task. The optimization of the separation and subsequent scale-up is usually carried out by trial and error. In this study, the relationship between retention parameters a and c for analytical and preparative separations was developed when the same solid adsorbent and mobile phase were used. The prediction and optimization of the preparative separation of a complex sample could be achieved by direct and simple conversion of the experimentally determined data from an analytical level. The novel method was successfully applied to optimize the separation of target compounds in traditional Chinese medicine (TCM). (C) 2008 Elsevier B.V. All rights reserved.
语种英语
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WOS记录号WOS:000253869900009
引用统计
被引频次:15[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/100093
专题中国科学院大连化学物理研究所
通讯作者Liang XM(梁鑫淼); Liang XM(梁鑫淼)
作者单位1.Chinese Acad Sci, Grad Sch, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
2.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China
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GB/T 7714
Jin, Yu,Xue, Xingya,Liu, Yanfang,et al. A novel method of prediction and optimization for preparative high-performance liquid chromatography separation[J]. JOURNAL OF CHROMATOGRAPHY A,2008,1183(1-2):76-86.
APA Jin, Yu.,Xue, Xingya.,Liu, Yanfang.,Xiao, Yuansheng.,Zhang, Jing.,...&梁鑫淼.(2008).A novel method of prediction and optimization for preparative high-performance liquid chromatography separation.JOURNAL OF CHROMATOGRAPHY A,1183(1-2),76-86.
MLA Jin, Yu,et al."A novel method of prediction and optimization for preparative high-performance liquid chromatography separation".JOURNAL OF CHROMATOGRAPHY A 1183.1-2(2008):76-86.
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