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Study on the retention equation in hydrophilic interaction liquid chromatography
Jin, Gaowa; Guo, Zhimou; Zhang, Feifang; Xue, Xingya; Jin, Yu; Liang, Xinmiao; Liang XM(梁鑫淼); Liang XM(梁鑫淼)
关键词Hydrophilic Interaction Liquid Chromatography Retention Equation Stationary Phases Selectivity Nucleoside
刊名TALANTA
2008-07-30
DOI10.1016/j.talanta.2008.03.042
76期:3页:522-527
收录类别SCI
文章类型Article
部门归属18
项目归属1803
产权排名1;1
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]ELECTROSPRAY MASS-SPECTROMETRY ; LIGHT-SCATTERING DETECTION ; SMALL POLAR COMPOUNDS ; REVERSED-PHASE ; ADRENORECEPTOR AGONISTS ; STATIONARY-PHASE ; DRUG DISCOVERY ; SEPARATION ; SILICA ; PERFORMANCE
英文摘要Hydrophilic interaction liquid chromatography (HILIC) is an effective technique for separating polar compounds. But its retention equation has not been studied systematically yet. in this study, an appropriate retention equation was established by using eight nucleosides as model analytes and by comparing four retention models on six different HILIC columns. As a result, retention equation In k = a + b x InCB + c x C-B could be quantitatively described the retention factors with good accuracy in HILIC mode. Based on this equation, the retention times of eight nucleosides under the conditions by other mobile phase can be predicted on each column. All of the predicted relative errors of retention times were smaller than 5%. The established retention model was also successfully applied to predict retention times of the real Traditional Chinese Medicine-Carthaus tinctorius L. sample. (C) 2008 Elsevier B.V. All rights reserved.
语种英语
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WOS记录号WOS:000257577100006
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被引频次:98[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/100097
专题中国科学院大连化学物理研究所
通讯作者Liang XM(梁鑫淼); Liang XM(梁鑫淼)
作者单位Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Liaoning, Peoples R China
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GB/T 7714
Jin, Gaowa,Guo, Zhimou,Zhang, Feifang,et al. Study on the retention equation in hydrophilic interaction liquid chromatography[J]. TALANTA,2008,76(3):522-527.
APA Jin, Gaowa.,Guo, Zhimou.,Zhang, Feifang.,Xue, Xingya.,Jin, Yu.,...&梁鑫淼.(2008).Study on the retention equation in hydrophilic interaction liquid chromatography.TALANTA,76(3),522-527.
MLA Jin, Gaowa,et al."Study on the retention equation in hydrophilic interaction liquid chromatography".TALANTA 76.3(2008):522-527.
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