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Synthesis and characterization of organic-functionalized molecular sieves Ph-SAPO-5 and Ph-SAPO-11
Zhou, D.1; Luo, X-B.1; Zhang, H-L.2; Dong, C.1; Xia, Q-H.1; Liu, Z-M.3; Deng, F.2; Xia QH(夏清华)
关键词Organic-functionalization Microporous Molecular Sieve Sapo-5 Sapo-11
刊名MICROPOROUS AND MESOPOROUS MATERIALS
2009-05-01
DOI10.1016/j.micromeso.2009.01.033
121期:1-3页:194-199
收录类别SCI
文章类型Article
部门归属12
项目归属12
产权排名3;6
WOS标题词Science & Technology ; Physical Sciences ; Technology
类目[WOS]Chemistry, Applied ; Chemistry, Physical ; Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
研究领域[WOS]Chemistry ; Science & Technology - Other Topics ; Materials Science
关键词[WOS]PERIODIC MESOPOROUS ORGANOSILICAS ; SOLID-STATE NMR ; INORGANIC HYBRID ZEOLITES ; FRAMEWORK ALUMINOPHOSPHATES ; CATALYTIC-PROPERTIES ; ACID ; SPECTROSCOPY ; DESIGN ; PHASES ; SILICA
英文摘要Organic-functionalized molecular sieves silicoaluminophosphates with AFI and AEL topologies have been first hydrothermally synthesized by using 1,4-bis(triethoxysilyl) benzene (BTEB) as unique silicon source. Various techniques have been performed to characterize the structures of the two molecular sieves. Powder XRD, solid-state (13)C CP/MAS NMR, FT-IR, UV-vis, and TGA analysis prove that there are aromatic groups in the final products, and (29)Si MAS NMR spectra demonstrate that two types of (29)Si chemical environments, i.e. organic T-type and inorganic Q-type silicon, coexist in the structures. The contents of organic groups are determined to be high up to 12 wt%. (C) 2009 Elsevier Inc. All rights reserved.
语种英语
原文出处查看原文
WOS记录号WOS:000265326400027
引用统计
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/102037
专题中国科学院大连化学物理研究所
通讯作者Xia QH(夏清华)
作者单位1.Hubei Univ, Minist Educ, Key Lab Synth & Applicat Organ Funct Mol, Wuhan 430062, Peoples R China
2.Chinese Acad Sci, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan Ctr Magnet Resonance, Wuhan 430071, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, Lab Nat Gas Utilizat & Appl Catalysis, Dalian 116023, Peoples R China
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Zhou, D.,Luo, X-B.,Zhang, H-L.,et al. Synthesis and characterization of organic-functionalized molecular sieves Ph-SAPO-5 and Ph-SAPO-11[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2009,121(1-3):194-199.
APA Zhou, D..,Luo, X-B..,Zhang, H-L..,Dong, C..,Xia, Q-H..,...&夏清华.(2009).Synthesis and characterization of organic-functionalized molecular sieves Ph-SAPO-5 and Ph-SAPO-11.MICROPOROUS AND MESOPOROUS MATERIALS,121(1-3),194-199.
MLA Zhou, D.,et al."Synthesis and characterization of organic-functionalized molecular sieves Ph-SAPO-5 and Ph-SAPO-11".MICROPOROUS AND MESOPOROUS MATERIALS 121.1-3(2009):194-199.
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