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题名: Synthesis and characterization of organic-functionalized molecular sieves Ph-SAPO-5 and Ph-SAPO-11
作者: Zhou, D.1;  Luo, X-B.1;  Zhang, H-L.2;  Dong, C.1;  Xia, Q-H.1;  Liu, Z-M.3;  Deng, F.2
通讯作者: 夏清华
关键词: Organic-functionalization ;  Microporous molecular sieve ;  SAPO-5 ;  SAPO-11
刊名: MICROPOROUS AND MESOPOROUS MATERIALS
发表日期: 2009-05-01
DOI: 10.1016/j.micromeso.2009.01.033
卷: 121, 期:1-3, 页:194-199
收录类别: SCI
文章类型: Article
部门归属: 12
项目归属: 12
产权排名: 3;6
WOS标题词: Science & Technology ;  Physical Sciences ;  Technology
类目[WOS]: Chemistry, Applied ;  Chemistry, Physical ;  Nanoscience & Nanotechnology ;  Materials Science, Multidisciplinary
研究领域[WOS]: Chemistry ;  Science & Technology - Other Topics ;  Materials Science
英文摘要: Organic-functionalized molecular sieves silicoaluminophosphates with AFI and AEL topologies have been first hydrothermally synthesized by using 1,4-bis(triethoxysilyl) benzene (BTEB) as unique silicon source. Various techniques have been performed to characterize the structures of the two molecular sieves. Powder XRD, solid-state (13)C CP/MAS NMR, FT-IR, UV-vis, and TGA analysis prove that there are aromatic groups in the final products, and (29)Si MAS NMR spectra demonstrate that two types of (29)Si chemical environments, i.e. organic T-type and inorganic Q-type silicon, coexist in the structures. The contents of organic groups are determined to be high up to 12 wt%. (C) 2009 Elsevier Inc. All rights reserved.
关键词[WOS]: PERIODIC MESOPOROUS ORGANOSILICAS ;  SOLID-STATE NMR ;  INORGANIC HYBRID ZEOLITES ;  FRAMEWORK ALUMINOPHOSPHATES ;  CATALYTIC-PROPERTIES ;  ACID ;  SPECTROSCOPY ;  DESIGN ;  PHASES ;  SILICA
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000265326400027
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/102037
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Hubei Univ, Minist Educ, Key Lab Synth & Applicat Organ Funct Mol, Wuhan 430062, Peoples R China
2.Chinese Acad Sci, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan Ctr Magnet Resonance, Wuhan 430071, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, Lab Nat Gas Utilizat & Appl Catalysis, Dalian 116023, Peoples R China

Recommended Citation:
Zhou, D.,Luo, X-B.,Zhang, H-L.,et al. Synthesis and characterization of organic-functionalized molecular sieves Ph-SAPO-5 and Ph-SAPO-11[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2009,121(1-3):194-199.
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