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Fingerprint analysis of Ligusticum chuanxiong using hydrophilic interaction chromatography and reversed-phase liquid chromatography
Jin, Yu1; Liang, Tu1; Fu, Qing1; Xiao, Yuan-Sheng1; Feng, Jia-Tao1; Ke, Yan-Xiong2; Liang, Xin-Miao1,2; Liang XM(梁鑫淼)
关键词Fingerprint Analysis Quality Control Ligusticum Chuanxiong Hydrophilic Interaction Chromatography (Hilic) Reversed-phase Liquid Chromatography (Rplc) Polar Compounds
刊名JOURNAL OF CHROMATOGRAPHY A
2009-03-13
DOI10.1016/j.chroma.2008.04.010
1216期:11页:2136-2141
收录类别SCI
文章类型Article
部门归属18
项目归属1803
产权排名1;1
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]ELECTROSPRAY MASS-SPECTROMETRY ; DIODE-ARRAY DETECTION ; QUALITY-CONTROL ; POLAR COMPOUNDS ; MEDICINAL-PLANTS ; HERBAL MEDICINES ; HPLC ; RHIZOMA ; DAD ; IDENTIFICATION
英文摘要Fingerprint analysis is considered one of the most powerful approaches to quality control in traditional Chinese medicines (TCMs). In this study, a binary chromatographic fingerprint analysis was developed using hydrophilic interaction chromatography (HILIC) and reversed-phase liquid chromatography (RPLC) to gain more chemical information about polar compounds and weakly polar compounds. This method was used to construct a chromatographic fingerprint of Ligusticum chuanxiong. The two chromatographic methods demonstrated good precision, reproducibility, and stability, with relative standard deviations of <2% for retention time and 7% for peak area for both HILIC and RPLC separations. Data from the analysis of 14 samples by HILIC and RPLC were processed with similarity analysis, with correlation coefficients and congruence coefficients. This binary fingerprint analysis, using two chromatographic modes, is a powerful tool for characterizing the quality of samples, and can be used for the comprehensive quality control of TCMs. (C) 2008 Elsevier B.V. All rights reserved.
语种英语
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WOS记录号WOS:000264226500021
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被引频次:53[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/102577
专题中国科学院大连化学物理研究所
通讯作者Liang XM(梁鑫淼)
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Grad Sch, Dalian 116023, Peoples R China
2.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China
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Jin, Yu,Liang, Tu,Fu, Qing,et al. Fingerprint analysis of Ligusticum chuanxiong using hydrophilic interaction chromatography and reversed-phase liquid chromatography[J]. JOURNAL OF CHROMATOGRAPHY A,2009,1216(11):2136-2141.
APA Jin, Yu.,Liang, Tu.,Fu, Qing.,Xiao, Yuan-Sheng.,Feng, Jia-Tao.,...&梁鑫淼.(2009).Fingerprint analysis of Ligusticum chuanxiong using hydrophilic interaction chromatography and reversed-phase liquid chromatography.JOURNAL OF CHROMATOGRAPHY A,1216(11),2136-2141.
MLA Jin, Yu,et al."Fingerprint analysis of Ligusticum chuanxiong using hydrophilic interaction chromatography and reversed-phase liquid chromatography".JOURNAL OF CHROMATOGRAPHY A 1216.11(2009):2136-2141.
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