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题名: Development of orthogonal two-dimensional hydrophilic interaction chromatography systems with the introduction of novel stationary phases
作者: Liu, Yanming1;  Guo, Zhimou1;  Feng, Jiatao1;  Xue, Xingya1;  Zhang, Feifang1;  Xu, Qing1;  Liang, Xinmiao1
通讯作者: 梁鑫淼
关键词: 2D-LC ;  High polarity ;  Orthogonality ;  Traditional Chinese medicine ;  Two-dimensional hydrophilic interaction chromatography
刊名: JOURNAL OF SEPARATION SCIENCE
发表日期: 2009-09-01
DOI: 10.1002/jssc.200900086
卷: 32, 期:17, 页:2871-2876
收录类别: SCI
文章类型: Article
部门归属: 18
项目归属: 1803
产权排名: 1;1
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical
研究领域[WOS]: Chemistry
英文摘要: Two different offline 2-D hydrophilic interaction chromatography (2D-HILIC/HILIC) systems have been developed. In the two systems, a click maltose column was used in the first dimension, an amide column or a click P-CD column was used in the second dimension, respectively. Both of the systems were used for the analysis of very polar components in Carthamus tinctorius Linn., which is a traditional Chinese medicine. Excellent orthogonality and separation results were obtained in both 2D-HILIC/HILIC systems, while the peak capacity of the system based on click maltose and amide column was higher for its adoption of stationary phase with smaller particle size in the second dimension.
关键词[WOS]: INTERACTION LIQUID-CHROMATOGRAPHY ;  TANDEM MASS-SPECTROMETRY ;  L. OIL CAKE ;  CARTHAMUS-TINCTORIUS ;  POLAR COMPOUNDS ;  SEPARATION ;  IDENTIFICATION
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000269780400003
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/102589
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Liaoning, Peoples R China

Recommended Citation:
Liu, Yanming,Guo, Zhimou,Feng, Jiatao,et al. Development of orthogonal two-dimensional hydrophilic interaction chromatography systems with the introduction of novel stationary phases[J]. JOURNAL OF SEPARATION SCIENCE,2009,32(17):2871-2876.
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