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题名: 2-D RP/RPLC method to separate components in Fructus schisandrae chinensis
作者: Jin, Gaowa1, 2;  Dai, Yuntao3;  Feng, Jiatao1;  Qin, Xuemei3;  Xue, Xingya1;  Zhang, Feifang1, 4;  Liang, Xinmiao1, 4
通讯作者: 章飞芳
关键词: beta-CD column ;  Fructus schisandrae chinensis ;  Traditional Chinese medicine ;  2-D RP/RPLC
刊名: JOURNAL OF SEPARATION SCIENCE
发表日期: 2010-03-01
DOI: 10.1002/jssc.200900563
卷: 33, 期:4-5, 页:564-569
收录类别: SCI
文章类型: Article
部门归属: 18
项目归属: 1803
产权排名: 1;1
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical
研究领域[WOS]: Chemistry
英文摘要: An off-line 2-D RP/RPLC method was developed to separate components in extracts of Fructus schisandrae chinensis, which is a traditional Chinese medicine. In this method, Click beta-CD stationary phase was proposed for constructing 2-D RP/RPLC system combined with C18 column. beta-CD column showed great potential to separate compounds in traditional Chinese medicines under RP mode. Collected fractions from Click beta-CD column used in first dimension were resolved into many additional components, indicating that the 2-D LC system based on Click beta-CD and C18 phases is orthogonal. The mobile phase was same on both columns. This 2-D LC method facilitates us not only to separate components that cannot be resolved by unidimensional chromatography, but also to achieve much more efficient detection of minor sample components.
关键词[WOS]: 2-DIMENSIONAL LIQUID-CHROMATOGRAPHY ;  HYDROPHILIC INTERACTION CHROMATOGRAPHY ;  RP-RP-HPLC ;  MASS-SPECTROMETRY ;  QUANTITATIVE-ANALYSIS ;  PHASE ;  CYCLODEXTRIN ;  PERFORMANCE ;  SYSTEM ;  CHEMISTRY
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000276573800014
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/103071
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.E China Univ Sci & Technol, Dalian Inst Chem Phys, Chinese Acad Sci, Key Lab Separat Sci Analyt Chem, Dalian 116023, Liaoning, Peoples R China
2.Chinese Acad Fishery Sci, E China Sea Fishery Res Inst, Shanghai, Peoples R China
3.Shanxi Univ, Modern Res Ctr Tradit Chinese Med, Taiyuan, Peoples R China
4.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China

Recommended Citation:
Jin, Gaowa,Dai, Yuntao,Feng, Jiatao,et al. 2-D RP/RPLC method to separate components in Fructus schisandrae chinensis[J]. JOURNAL OF SEPARATION SCIENCE,2010,33(4-5):564-569.
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