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2-D RP/RPLC method to separate components in Fructus schisandrae chinensis
Jin, Gaowa1,2; Dai, Yuntao3; Feng, Jiatao1; Qin, Xuemei3; Xue, Xingya1; Zhang, Feifang1,4; Liang, Xinmiao1,4; Zhang FF(章飞芳)
关键词Beta-cd Column Fructus Schisandrae Chinensis Traditional Chinese Medicine 2-d Rp/rplc
刊名JOURNAL OF SEPARATION SCIENCE
2010-03-01
DOI10.1002/jssc.200900563
33期:4-5页:564-569
收录类别SCI
文章类型Article
部门归属18
项目归属1803
产权排名1;1
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]2-DIMENSIONAL LIQUID-CHROMATOGRAPHY ; HYDROPHILIC INTERACTION CHROMATOGRAPHY ; RP-RP-HPLC ; MASS-SPECTROMETRY ; QUANTITATIVE-ANALYSIS ; PHASE ; CYCLODEXTRIN ; PERFORMANCE ; SYSTEM ; CHEMISTRY
英文摘要An off-line 2-D RP/RPLC method was developed to separate components in extracts of Fructus schisandrae chinensis, which is a traditional Chinese medicine. In this method, Click beta-CD stationary phase was proposed for constructing 2-D RP/RPLC system combined with C18 column. beta-CD column showed great potential to separate compounds in traditional Chinese medicines under RP mode. Collected fractions from Click beta-CD column used in first dimension were resolved into many additional components, indicating that the 2-D LC system based on Click beta-CD and C18 phases is orthogonal. The mobile phase was same on both columns. This 2-D LC method facilitates us not only to separate components that cannot be resolved by unidimensional chromatography, but also to achieve much more efficient detection of minor sample components.
语种英语
原文出处查看原文
WOS记录号WOS:000276573800014
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/103071
专题中国科学院大连化学物理研究所
通讯作者Zhang FF(章飞芳)
作者单位1.E China Univ Sci & Technol, Dalian Inst Chem Phys, Chinese Acad Sci, Key Lab Separat Sci Analyt Chem, Dalian 116023, Liaoning, Peoples R China
2.Chinese Acad Fishery Sci, E China Sea Fishery Res Inst, Shanghai, Peoples R China
3.Shanxi Univ, Modern Res Ctr Tradit Chinese Med, Taiyuan, Peoples R China
4.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China
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Jin, Gaowa,Dai, Yuntao,Feng, Jiatao,et al. 2-D RP/RPLC method to separate components in Fructus schisandrae chinensis[J]. JOURNAL OF SEPARATION SCIENCE,2010,33(4-5):564-569.
APA Jin, Gaowa.,Dai, Yuntao.,Feng, Jiatao.,Qin, Xuemei.,Xue, Xingya.,...&章飞芳.(2010).2-D RP/RPLC method to separate components in Fructus schisandrae chinensis.JOURNAL OF SEPARATION SCIENCE,33(4-5),564-569.
MLA Jin, Gaowa,et al."2-D RP/RPLC method to separate components in Fructus schisandrae chinensis".JOURNAL OF SEPARATION SCIENCE 33.4-5(2010):564-569.
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