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2-D RP/RPLC method to separate components in Fructus schisandrae chinensis
Jin, Gaowa1,2; Dai, Yuntao3; Feng, Jiatao1; Qin, Xuemei3; Xue, Xingya1; Zhang, Feifang1,4; Liang, Xinmiao1,4; Zhang FF(章飞芳)
KeywordBeta-cd Column Fructus Schisandrae Chinensis Traditional Chinese Medicine 2-d Rp/rplc
Source PublicationJOURNAL OF SEPARATION SCIENCE
2010-03-01
DOI10.1002/jssc.200900563
Volume33Issue:4-5Pages:564-569
Indexed BySCI
SubtypeArticle
Department18
Funding Project1803
Contribution Rank1;1
WOS HeadingsScience & Technology ; Physical Sciences
WOS SubjectChemistry, Analytical
WOS Research AreaChemistry
WOS Keyword2-DIMENSIONAL LIQUID-CHROMATOGRAPHY ; HYDROPHILIC INTERACTION CHROMATOGRAPHY ; RP-RP-HPLC ; MASS-SPECTROMETRY ; QUANTITATIVE-ANALYSIS ; PHASE ; CYCLODEXTRIN ; PERFORMANCE ; SYSTEM ; CHEMISTRY
AbstractAn off-line 2-D RP/RPLC method was developed to separate components in extracts of Fructus schisandrae chinensis, which is a traditional Chinese medicine. In this method, Click beta-CD stationary phase was proposed for constructing 2-D RP/RPLC system combined with C18 column. beta-CD column showed great potential to separate compounds in traditional Chinese medicines under RP mode. Collected fractions from Click beta-CD column used in first dimension were resolved into many additional components, indicating that the 2-D LC system based on Click beta-CD and C18 phases is orthogonal. The mobile phase was same on both columns. This 2-D LC method facilitates us not only to separate components that cannot be resolved by unidimensional chromatography, but also to achieve much more efficient detection of minor sample components.
Language英语
URL查看原文
WOS IDWOS:000276573800014
Citation statistics
Cited Times:9[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/103071
Collection中国科学院大连化学物理研究所
Corresponding AuthorZhang FF(章飞芳)
Affiliation1.E China Univ Sci & Technol, Dalian Inst Chem Phys, Chinese Acad Sci, Key Lab Separat Sci Analyt Chem, Dalian 116023, Liaoning, Peoples R China
2.Chinese Acad Fishery Sci, E China Sea Fishery Res Inst, Shanghai, Peoples R China
3.Shanxi Univ, Modern Res Ctr Tradit Chinese Med, Taiyuan, Peoples R China
4.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China
Recommended Citation
GB/T 7714
Jin, Gaowa,Dai, Yuntao,Feng, Jiatao,et al. 2-D RP/RPLC method to separate components in Fructus schisandrae chinensis[J]. JOURNAL OF SEPARATION SCIENCE,2010,33(4-5):564-569.
APA Jin, Gaowa.,Dai, Yuntao.,Feng, Jiatao.,Qin, Xuemei.,Xue, Xingya.,...&章飞芳.(2010).2-D RP/RPLC method to separate components in Fructus schisandrae chinensis.JOURNAL OF SEPARATION SCIENCE,33(4-5),564-569.
MLA Jin, Gaowa,et al."2-D RP/RPLC method to separate components in Fructus schisandrae chinensis".JOURNAL OF SEPARATION SCIENCE 33.4-5(2010):564-569.
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