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学科主题: 物理化学
题名: Preparation and application of organic-silica hybrid monolithic capillary columns
作者: Wu, Minghuo1, 2;  Wu, Ren'an1;  Zhang, Zhenbin1, 2;  Zou, Hanfa1
通讯作者: 邹汉法
关键词: CEC ;  Enzymatic reactor ;  Hybrid monolith ;  Micro-HPLC ;  SPME
刊名: ELECTROPHORESIS
发表日期: 2011
DOI: 10.1002/elps.201000349
卷: 32, 期:1, 页:105-115
收录类别: SCI
文章类型: Review
部门归属: 18
项目归属: 1809
产权排名: 1,1
WOS标题词: Science & Technology ;  Life Sciences & Biomedicine ;  Physical Sciences
类目[WOS]: Biochemical Research Methods ;  Chemistry, Analytical
摘要: Preparation and application of organic-silica hybrid monolithic capillary columns
研究领域[WOS]: Biochemistry & Molecular Biology ;  Chemistry
英文摘要: Organic-silica hybrid monolithic columns have drawn more and more attention due to the ease of preparation and good mechanical stability in recent years. Many synthetic approaches have been developed and a variety of hybrid monolithic capillary columns have been prepared. The sol-gel process is well recognized in the fabrication of hybrid monolithic columns, which can be mainly classified as one-step, acid/base two-step procedures. The new approaches such as the " one-pot'' and nano-scaled inorganic-organic hybrid reagent of polyhedral oligomeric silsesquioxane used as a cross-linker have also emerged for the preparation of hybrid monolithic columns. The applications of the organic-silica hybrid monolithic capillary columns for capillary electrochromatography, micro high-performance liquid chromatography, solid-phase microextraction and enzymatic reactor etc. are included in this review.
关键词[WOS]: POLYHEDRAL OLIGOMERIC SILSESQUIOXANE ;  PERFORMANCE LIQUID-CHROMATOGRAPHY ;  SOL-GEL METHOD ;  STATIONARY PHASES ;  HIGH-EFFICIENCY ;  AFFINITY-CHROMATOGRAPHY ;  ELECTROOSMOTIC FLOW ;  STEP SYNTHESIS ;  ELECTROCHROMATOGRAPHY ;  EXCHANGE
语种: 英语
WOS记录号: WOS:000285425000010
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/115187
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, CAS Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing, Peoples R China

Recommended Citation:
Wu, Minghuo,Wu, Ren'an,Zhang, Zhenbin,et al. Preparation and application of organic-silica hybrid monolithic capillary columns[J]. ELECTROPHORESIS,2011,32(1):105-115.
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