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学科主题物理化学
Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs
Jiang, Chun-Hong1,2; Song, Li-Fang1,2; Jiao, Cheng-Li1,2; Zhang, Jian1; Sun, Li-Xian1; Xu, Fen3; Zhang, Huan-Zhi1; Xu, Qing-Yang1; Gabelica, Zelimir4; Sun LX(孙立贤); XuFen
关键词Ca-mof Mn-ii-mof Molar Heat Capacity Tg Temperature-modulated Dsc
刊名JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
2011-03-01
ISSN1388-6150
DOI10.1007/s10973-010-1197-7
103期:3页:1095-1103
收录类别SCI
文章类型Article
部门归属DNL19
项目归属1903
产权排名1,1
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical ; Chemistry, Physical
研究领域[WOS]Chemistry
关键词[WOS]METAL-ORGANIC FRAMEWORKS ; HYDROGEN SORPTION ; GAS-ADSORPTION ; PHOTOLUMINESCENCE ; STORAGE ; SEPARATION ; CATALYSTS ; CO2
英文摘要Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs; Two metal-organic frameworks, Ca(2,6-NDC)(DMF) (1) and Mn-3(2,6-NDC)(3)(DMF)(4) (2) (where 2,6-NDC = 2,6-naphthalene dicarboxylate and DMF = N,N'-dimethylformamide) have been solvothermally synthesized under optimized conditions and characterized by X-ray powder diffraction, elemental analysis, FT-IR spectroscopy, and TG analysis. The thermal decomposition characteristics were investigated under air atmosphere from 300 to 1,170 K (for 1) and from 300 to 971 K (for 2). The molar heat capacities were measured from 198 to 548 K (for 1) and from 198 to 448 K (for 2) by temperature modulated differential scanning calorimetry (TMDSC) for the first time. The fundamental thermodynamic parameters such as entropy and enthalpy variations with temperature were calculated based on the experimentally determined molar heat capacities.
语种英语
WOS记录号WOS:000287712400040
引用统计
被引频次:10[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/115776
专题中国科学院大连化学物理研究所
通讯作者Sun LX(孙立贤); XuFen
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
3.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China
4.Univ Haute Alsace, ENSCMu, Lab LPI GSEC, F-68094 Mulhouse, France
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Jiang, Chun-Hong,Song, Li-Fang,Jiao, Cheng-Li,et al. Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs[J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,2011,103(3):1095-1103.
APA Jiang, Chun-Hong.,Song, Li-Fang.,Jiao, Cheng-Li.,Zhang, Jian.,Sun, Li-Xian.,...&XuFen.(2011).Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs.JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,103(3),1095-1103.
MLA Jiang, Chun-Hong,et al."Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs".JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY 103.3(2011):1095-1103.
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