DICP OpenIR
Subject Area物理化学
Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs
Jiang, Chun-Hong1,2; Song, Li-Fang1,2; Jiao, Cheng-Li1,2; Zhang, Jian1; Sun, Li-Xian1; Xu, Fen3; Zhang, Huan-Zhi1; Xu, Qing-Yang1; Gabelica, Zelimir4; Sun LX(孙立贤); XuFen
KeywordCa-mof Mn-ii-mof Molar Heat Capacity Tg Temperature-modulated Dsc
Source PublicationJOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
2011-03-01
ISSN1388-6150
DOI10.1007/s10973-010-1197-7
Volume103Issue:3Pages:1095-1103
Indexed BySCI
SubtypeArticle
DepartmentDNL19
Funding Project1903
Contribution Rank1,1
WOS HeadingsScience & Technology ; Physical Sciences
WOS SubjectChemistry, Analytical ; Chemistry, Physical
WOS Research AreaChemistry
WOS KeywordMETAL-ORGANIC FRAMEWORKS ; HYDROGEN SORPTION ; GAS-ADSORPTION ; PHOTOLUMINESCENCE ; STORAGE ; SEPARATION ; CATALYSTS ; CO2
AbstractDetermination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs; Two metal-organic frameworks, Ca(2,6-NDC)(DMF) (1) and Mn-3(2,6-NDC)(3)(DMF)(4) (2) (where 2,6-NDC = 2,6-naphthalene dicarboxylate and DMF = N,N'-dimethylformamide) have been solvothermally synthesized under optimized conditions and characterized by X-ray powder diffraction, elemental analysis, FT-IR spectroscopy, and TG analysis. The thermal decomposition characteristics were investigated under air atmosphere from 300 to 1,170 K (for 1) and from 300 to 971 K (for 2). The molar heat capacities were measured from 198 to 548 K (for 1) and from 198 to 448 K (for 2) by temperature modulated differential scanning calorimetry (TMDSC) for the first time. The fundamental thermodynamic parameters such as entropy and enthalpy variations with temperature were calculated based on the experimentally determined molar heat capacities.
Language英语
WOS IDWOS:000287712400040
Citation statistics
Cited Times:12[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/115776
Collection中国科学院大连化学物理研究所
Corresponding AuthorSun LX(孙立贤); XuFen
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
3.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China
4.Univ Haute Alsace, ENSCMu, Lab LPI GSEC, F-68094 Mulhouse, France
Recommended Citation
GB/T 7714
Jiang, Chun-Hong,Song, Li-Fang,Jiao, Cheng-Li,et al. Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs[J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,2011,103(3):1095-1103.
APA Jiang, Chun-Hong.,Song, Li-Fang.,Jiao, Cheng-Li.,Zhang, Jian.,Sun, Li-Xian.,...&XuFen.(2011).Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs.JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,103(3),1095-1103.
MLA Jiang, Chun-Hong,et al."Determination of heat capacities and thermodynamic properties of two structurally unrelated but isotypic calcium and manganese(II) 2,6-naphthalene dicarboxylate-based MOFs".JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY 103.3(2011):1095-1103.
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