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学科主题: 物理化学
题名: Exceptional thermal stability and thermodynamic properties of lithium based metal-organic framework
作者: Jiang, Chun-Hong1, 3;  Song, Li-Fang1, 3;  Jiao, Cheng-Li1, 3;  Zhang, Jian1;  Sun, Li-Xian1;  Xu, Fen2;  Du, Yong4;  Cao, Zhong5
通讯作者: 孙立贤
关键词: Lithium ;  Molar heat capacity ;  Metal-organic frameworks ;  TG ;  TMDSC
刊名: JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
发表日期: 2011
DOI: 10.1007/s10973-010-0880-z
卷: 103, 期:1, 页:373-380
收录类别: SCI
文章类型: Article
部门归属: DNL19
项目归属: 1903
产权排名: 1,1
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical ;  Chemistry, Physical
摘要: Exceptional thermal stability and thermodynamic properties of lithium based metal-organic framework
研究领域[WOS]: Chemistry
英文摘要: A three-dimensional lithium-based metal-organic framework Li-2(2,6-NDC) ( 2,6-NDC = 2,6-naphthalene dicarboxylate) has been synthesized solvothermally and characterized by X-ray powder diffraction, elemental analysis, FT-IR spectroscopy, thermogravimetry and mass spectrometer analysis (TG-MS). The framework has exceptional stability and is stable to 863 K. The thermal decomposition characteristic of this compound was investigated through the TG-MS from 293 to 1250 K. The molar heat capacity of the compound was measured by temperature modulated differential scanning calorimetry (TMDSC) over the temperature range from 195 to 670 K for the first time. The thermodynamic parameters such as entropy and enthalpy versus 298.15 K based on the above molar heat capacity were calculated.
关键词[WOS]: HEAT-CAPACITY ;  COORDINATION POLYMER ;  PHOTOLUMINESCENCE ;  SEPARATION ;  CATALYSIS ;  MIXTURES ;  PRESSURE ;  STORAGE ;  H-2 ;  CH4
语种: 英语
WOS记录号: WOS:000287714400054
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/115779
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China
2.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China
3.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
4.Cent S Univ, State Key Lab Powder Met, Changsha 410083, Peoples R China
5.Changsha Univ Sci & Technol, Sch Chem & Environm Engn, Changsha 410076, Hunan, Peoples R China

Recommended Citation:
Jiang, Chun-Hong,Song, Li-Fang,Jiao, Cheng-Li,et al. Exceptional thermal stability and thermodynamic properties of lithium based metal-organic framework[J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,2011,103(1):373-380.
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