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学科主题: 物理化学
题名: Recent advances in preparation and application of hybrid organic-silica monolithic capillary columns
作者: Ou, Junjie1;  Lin, Hui1, 2;  Zhang, Zhenbin1, 2;  Huang, Guang1, 3;  Dong, Jing1;  Zou, Hanfa1
通讯作者: 欧俊杰
关键词: Monolithic columns ;  Organic-silica hybrid materials ;  Ring-opening polymerization ;  Sol-gel
刊名: ELECTROPHORESIS
发表日期: 2013
DOI: 10.1002/elps.201200344
卷: 34, 期:1, 页:126-140
收录类别: SCI
文章类型: Review
部门归属: 18
项目归属: 1809
产权排名: 1,1
WOS标题词: Science & Technology ;  Life Sciences & Biomedicine ;  Physical Sciences
类目[WOS]: Biochemical Research Methods ;  Chemistry, Analytical
研究领域[WOS]: Biochemistry & Molecular Biology ;  Chemistry
英文摘要: Hybrid organic-silica monolithic columns, regarded as a second generation of silica-based monoliths, have received much interest due to their unique properties over the pure silica-based monoliths. This review mainly focuses on development in the fields of preparation of hybrid monolithic columns in a capillary and their application for CEC and capillary liquid chromatography separation, as well as for sample pretreatment of solid-phase microextraction and immobilized enzyme reactor since July 2010. The preparation approaches are comprehensively summarized with three routes: (i) general solgel process using trialkoxysilanes and tetraalkoxysilanes as coprecursors; (ii) one-pot process of alkoxysilanes and organic monomers concomitantly proceeding solgel chemistry and free radical polymerization; and (iii) other polymerization approaches of organic monomers containing silanes. The modification of hybrid monoliths containing reactive groups to acquire the desired surface functionality is also described.
关键词[WOS]: PERFORMANCE LIQUID-CHROMATOGRAPHY ;  OPENING METATHESIS POLYMERIZATION ;  MOLECULARLY IMPRINTED POLYMER ;  PLASMA-MASS SPECTROMETRY ;  LESS COMMON APPLICATIONS ;  ONE-POT APPROACH ;  SOL-GEL METHOD ;  STATIONARY PHASES ;  REVERSED-PHASE ;  CLICK CHEMISTRY
语种: 英语
WOS记录号: WOS:000313123100011
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/117615
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, CAS Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing, Peoples R China
3.Dalian Univ Technol, Dalian, Peoples R China

Recommended Citation:
Ou, Junjie,Lin, Hui,Zhang, Zhenbin,et al. Recent advances in preparation and application of hybrid organic-silica monolithic capillary columns[J]. ELECTROPHORESIS,2013,34(1):126-140.
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