DICP OpenIR
Subject Area物理化学
Layered precursors for new zeolitic materials: Synthesis and characterization of B-RUB-39 and its condensation product B-RUB-41
Gruenewald-Lueke, Antje1; Gies, Hermann1; Mueller, Ulrich2; Yilmaz, Bilge2; Imai, H.3; Tatsumi, Takashi3; Xie, B.4; Xiao, Feng-Shou4; Bao, Xinhe5; Zhang, Weiping5; De Vos, Dirk6; AntjeGrunewaldLuke
KeywordRro Framework Type B-substitution Rietveld Structure Analysis Rub-41 Topotactic Condensation Of Layered Precursors
Source PublicationMICROPOROUS AND MESOPOROUS MATERIALS
2012
DOI10.1016/j.micromeso.2011.05.036
Volume147Issue:1Pages:102-109
Indexed BySCI
SubtypeArticle
Department5
Funding Project502
Contribution Rank5,9
WOS HeadingsScience & Technology ; Physical Sciences ; Technology
WOS SubjectChemistry, Applied ; Chemistry, Physical ; Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
WOS Research AreaChemistry ; Science & Technology - Other Topics ; Materials Science
WOS KeywordTOPOTACTIC CONDENSATION ; SILICATE ; BORON ; TITANOSILICATE ; EPOXIDATION ; NMR
AbstractCondensation of layered silicate precursors leads to new, all silica zeolite frameworks. In order to introduce catalytic functionality, boron has been substituted into the silicate layer of RUB-39 in a single step synthesis process. Condensation of the silicate layer to the zeolite framework of RUB-41. RRO framework structure type, preserved B as constituent of the material. Analysis of structural details obtained from Rietveld analysis of powder diffraction data, (11)B and (29)Si NMR experiments of the as synthesized precursor as well as of the zeolite condensation product, and crystal chemical reasoning indicates segregation of B on one specific T-site. This T-site is buried in the silicate anionic layer of the precursor shielding the additional negative charge introduced by the trivalent T-atom. (C) 2011 Elsevier Inc. All rights reserved.
Language英语
WOS IDWOS:000295906200014
Citation statistics
Cited Times:11[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/118510
Collection中国科学院大连化学物理研究所
Corresponding AuthorAntjeGrunewaldLuke
Affiliation1.Ruhr Univ Bochum, Inst f Geol Mineral & Geophys, D-44780 Bochum, Germany
2.BASF SE, D-67056 Ludwigshafen, Germany
3.Tokyo Inst Technol, Chem Resources Lab, Yokohama, Kanagawa 227, Japan
4.Zhejiang Univ, Dept Chem, Hangzhou 310003, Zhejiang, Peoples R China
5.Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian, Peoples R China
6.Katholieke Univ Leuven, Ctr Surface Chem & Catalysis, Louvain, Belgium
Recommended Citation
GB/T 7714
Gruenewald-Lueke, Antje,Gies, Hermann,Mueller, Ulrich,et al. Layered precursors for new zeolitic materials: Synthesis and characterization of B-RUB-39 and its condensation product B-RUB-41[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2012,147(1):102-109.
APA Gruenewald-Lueke, Antje.,Gies, Hermann.,Mueller, Ulrich.,Yilmaz, Bilge.,Imai, H..,...&AntjeGrunewaldLuke.(2012).Layered precursors for new zeolitic materials: Synthesis and characterization of B-RUB-39 and its condensation product B-RUB-41.MICROPOROUS AND MESOPOROUS MATERIALS,147(1),102-109.
MLA Gruenewald-Lueke, Antje,et al."Layered precursors for new zeolitic materials: Synthesis and characterization of B-RUB-39 and its condensation product B-RUB-41".MICROPOROUS AND MESOPOROUS MATERIALS 147.1(2012):102-109.
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