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学科主题物理化学
Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)
Zhou, Yi-Xi1,2; Sun, Li-Xian1; Cao, Zhong2; Xu, Fen3; Jiang, Chun-Hong1; Jiao, Cheng-Li1; Zhang, Hui1,2; Zhang, Jian1; Zhou, Huai-Ying4; Li, Fen1; Zhao, Zi-Ming1; Zhang, Huang-Zhi1; Sun LX(孙立贤)
关键词Crystalline Molar Heat Capacity Tg Tmdsc
刊名JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
2013-02-01
DOI10.1007/s10973-012-2475-3
111期:2页:1603-1608
收录类别SCI
合作性质
文章类型Article
部门归属DNL19
项目归属DNL1903
产权排名待补充
WOS标题词Science & Technology ; Physical Sciences
资助者1,1 ; 1,1 ; 1,1 ; 1,1
类目[WOS]Chemistry, Analytical ; Chemistry, Physical
研究领域[WOS]Chemistry
关键词[WOS]STORAGE MATERIALS ; DSC ; NANOSTRUCTURES ; TEMPERATURE ; POLYMER
英文摘要The low-temperature molar heat capacity of crystalline Ni-9(btz)(12)(DMA)(6)(NO3)(6) (1) (btz = benzotriazolate; DMA = N,N'-dimethylacetamide) was measured by temperature-modulated differential scanning calorimetry for the first time. The thermodynamic parameters such as entropy and enthalpy relative to reference temperature 298.15 K were obtained based on the above molar heat capacity data. The compound was synthesized by solvothermal method and characterized by powder X-ray diffraction and FT-IR spectra. Moreover, the thermal stability and the decomposition mechanism of Ni-9(btz)(12)(DMA)(6)(NO3)(6) were investigated by thermogravimetry (TG) analysis under air atmosphere from 300 to 873 K. The experimental results through TG measurement demonstrate that the compound has a two-stage mass loss in air flow.
语种英语
资助者1,1 ; 1,1 ; 1,1 ; 1,1
原文出处查看原文
WOS记录号WOS:000313409700077
引用统计
被引频次:2[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/119236
专题中国科学院大连化学物理研究所
通讯作者Sun LX(孙立贤)
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China
2.Changsha Univ Sci & Technol, Sch Chem & Biol Engn, Changsha 410004, Hunan, Peoples R China
3.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China
4.Guilin Univ Elect Technol, Dept Mat Sci & Engn, Guilin 541004, Peoples R China
推荐引用方式
GB/T 7714
Zhou, Yi-Xi,Sun, Li-Xian,Cao, Zhong,et al. Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)[J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,2013,111(2):1603-1608.
APA Zhou, Yi-Xi.,Sun, Li-Xian.,Cao, Zhong.,Xu, Fen.,Jiang, Chun-Hong.,...&孙立贤.(2013).Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6).JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,111(2),1603-1608.
MLA Zhou, Yi-Xi,et al."Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)".JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY 111.2(2013):1603-1608.
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