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学科主题: 物理化学
题名: Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)
作者: Zhou, Yi-Xi1, 2;  Sun, Li-Xian1;  Cao, Zhong2;  Xu, Fen3;  Jiang, Chun-Hong1;  Jiao, Cheng-Li1;  Zhang, Hui1, 2;  Zhang, Jian1;  Zhou, Huai-Ying4;  Li, Fen1;  Zhao, Zi-Ming1;  Zhang, Huang-Zhi1
通讯作者: 孙立贤
关键词: Crystalline ;  Molar heat capacity ;  TG ;  TMDSC
刊名: JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
发表日期: 2013-02-01
DOI: 10.1007/s10973-012-2475-3
卷: 111, 期:2, 页:1603-1608
收录类别: SCI
合作性质: 
文章类型: Article
部门归属: DNL19
项目归属: DNL1903
产权排名: 待补充
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical ;  Chemistry, Physical
资助者: 1,1
研究领域[WOS]: Chemistry
英文摘要: The low-temperature molar heat capacity of crystalline Ni-9(btz)(12)(DMA)(6)(NO3)(6) (1) (btz = benzotriazolate; DMA = N,N'-dimethylacetamide) was measured by temperature-modulated differential scanning calorimetry for the first time. The thermodynamic parameters such as entropy and enthalpy relative to reference temperature 298.15 K were obtained based on the above molar heat capacity data. The compound was synthesized by solvothermal method and characterized by powder X-ray diffraction and FT-IR spectra. Moreover, the thermal stability and the decomposition mechanism of Ni-9(btz)(12)(DMA)(6)(NO3)(6) were investigated by thermogravimetry (TG) analysis under air atmosphere from 300 to 873 K. The experimental results through TG measurement demonstrate that the compound has a two-stage mass loss in air flow.
关键词[WOS]: STORAGE MATERIALS ;  DSC ;  NANOSTRUCTURES ;  TEMPERATURE ;  POLYMER
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000313409700077
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/119236
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China
2.Changsha Univ Sci & Technol, Sch Chem & Biol Engn, Changsha 410004, Hunan, Peoples R China
3.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China
4.Guilin Univ Elect Technol, Dept Mat Sci & Engn, Guilin 541004, Peoples R China

Recommended Citation:
Zhou, Yi-Xi,Sun, Li-Xian,Cao, Zhong,et al. Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)[J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,2013,111(2):1603-1608.
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