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学科主题: 物理化学
题名: Heat capacities and thermodynamic properties of Co(3,5-PDC)(H2O)
作者: Jiang, Xia1, 2;  Jiao, Cheng-Li1, 2;  Sun, Yu-Jia3;  Li, Zhi-Bao1, 2;  Liu, Shuang1, 2;  Zhang, Jian1;  Wang, Zi-Qiang1, 2;  Sun, Li-Xian1, 4;  Xu, Fen5;  Zhou, Huai-Ying4;  Sawada, Yutaka6
通讯作者: 孙立贤
关键词: 3,5-PDC ;  Metal-organic frameworks ;  Molar heat capacity ;  TG ;  TMDSC
刊名: JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
发表日期: 2013-06-01
DOI: 10.1007/s10973-012-2737-0
卷: 112, 期:3, 页:1579-1585
收录类别: SCI
合作性质: 
文章类型: Article
部门归属: DNL19
项目归属: DNL1903
产权排名: 待补充
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical ;  Chemistry, Physical
资助者: 1,1
研究领域[WOS]: Chemistry
英文摘要: A novel metal-organic frameworks Co(3,5-PDC)(H2O) (CoMOF, 3,5-PDC = pyridine-3,5-dicarboxylic acid) has been synthesized hydrothermally and characterized by single-crystal XRD and FT-IR spectra. The thermal stability and the decomposition mechanism of CoMOF were investigated by thermogravimetry-mass spectrometry, and a two-stage shape curve of mass loss was observed. Moreover, the low-temperature molar heat capacities were measured by temperature-modulated differential scanning calorimetry for the first time. The thermodynamic parameters such as entropy and enthalpy relative to reference temperature 298.15 K were derived based on the molar heat capacity data.
关键词[WOS]: METAL-ORGANIC-FRAMEWORK ;  COORDINATION POLYMERS ;  ADSORPTION
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000319358500053
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/119688
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
3.Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China
4.Guilin Univ Elect Technol, Dept Mat Sci & Engn, Guilin 541004, Peoples R China
5.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China
6.Tokyo Polytech Univ, Ctr Hyper Media Res, Grad Sch Engn, Atsugi, Kanagawa, Japan

Recommended Citation:
Jiang, Xia,Jiao, Cheng-Li,Sun, Yu-Jia,et al. Heat capacities and thermodynamic properties of Co(3,5-PDC)(H2O)[J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,2013,112(3):1579-1585.
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