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题名: Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices
作者: Teng Man1, 2;  Jin Jing3;  Fu Qiang2;  Cai YaQi1;  Chen JiPing3;  Wei FuSheng1, 2
关键词: hexabromocyclododecane ;  polychlorinated naphthalene ;  selective separation ;  tetrabromobisphenol A
刊名: CHINESE SCIENCE BULLETIN
发表日期: 2013-02-01
DOI: 10.1007/s11434-012-5638-5
卷: 58, 期:4-5, 页:500-506
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Multidisciplinary Sciences
研究领域[WOS]: Science & Technology - Other Topics
英文摘要: A method for the selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in complex matrices was developed. In the present study, the type of sorbents and the volume and composition of eluting solvents were investigated in detail. Under the optimal conditions, the recoveries of PCNs, HBCDs and TBBPA in different fractions were determined with liquid/gas chromatography tandem mass spectrometry (LC or GC-MS/MS), which was nearly close to 100%. To investigate the feasibility of the developed method, it was applied to isolate target compounds from spiked soil extracts. PCNs, HBCDs and TBBPA could be subsequently eluted with hexane, hexane/dichloromethane (1: 1), and hexane/dichloromethane (1: 3), and the recoveries of the analysts from three fractions were satisfactory (70.9%-107%) with the exception of gamma-HBCD at low levels. The results indicated that the method exhibited good performance for the selective separation of PCNs, HBCDs and TBBPA and showed great potential in sample pretreatment in terms of alleviating influence from different class of impurities to some extent.
关键词[WOS]: BROMINATED FLAME RETARDANTS ;  POLYBROMINATED DIPHENYL ETHERS ;  TANDEM MASS-SPECTROMETRY ;  THERMAL-STABILITY ;  SEWAGE-SLUDGE ;  SEDIMENTS ;  ATMOSPHERE ;  CHINA ;  WATER ;  PCBS
语种: 英语
WOS记录号: WOS:000315445500010
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/137944
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Res Ctr Ecoenvironm Sci, Beijing 100085, Peoples R China
2.China Natl Environm Monitoring Ctr, Beijing 100012, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China

Recommended Citation:
Teng Man,Jin Jing,Fu Qiang,et al. Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices[J]. CHINESE SCIENCE BULLETIN,2013,58(4-5):500-506.
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