DICP OpenIR
Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices
Teng Man1,2; Jin Jing3; Fu Qiang2; Cai YaQi1; Chen JiPing3; Wei FuSheng1,2
KeywordHexabromocyclododecane Polychlorinated Naphthalene Selective Separation Tetrabromobisphenol a
Source PublicationCHINESE SCIENCE BULLETIN
2013-02-01
DOI10.1007/s11434-012-5638-5
Volume58Issue:4-5Pages:500-506
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology
WOS SubjectMultidisciplinary Sciences
WOS Research AreaScience & Technology - Other Topics
WOS KeywordBROMINATED FLAME RETARDANTS ; POLYBROMINATED DIPHENYL ETHERS ; TANDEM MASS-SPECTROMETRY ; THERMAL-STABILITY ; SEWAGE-SLUDGE ; SEDIMENTS ; ATMOSPHERE ; CHINA ; WATER ; PCBS
AbstractA method for the selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in complex matrices was developed. In the present study, the type of sorbents and the volume and composition of eluting solvents were investigated in detail. Under the optimal conditions, the recoveries of PCNs, HBCDs and TBBPA in different fractions were determined with liquid/gas chromatography tandem mass spectrometry (LC or GC-MS/MS), which was nearly close to 100%. To investigate the feasibility of the developed method, it was applied to isolate target compounds from spiked soil extracts. PCNs, HBCDs and TBBPA could be subsequently eluted with hexane, hexane/dichloromethane (1: 1), and hexane/dichloromethane (1: 3), and the recoveries of the analysts from three fractions were satisfactory (70.9%-107%) with the exception of gamma-HBCD at low levels. The results indicated that the method exhibited good performance for the selective separation of PCNs, HBCDs and TBBPA and showed great potential in sample pretreatment in terms of alleviating influence from different class of impurities to some extent.
Language英语
WOS IDWOS:000315445500010
Citation statistics
Cited Times:2[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/137944
Collection中国科学院大连化学物理研究所
Affiliation1.Chinese Acad Sci, Res Ctr Ecoenvironm Sci, Beijing 100085, Peoples R China
2.China Natl Environm Monitoring Ctr, Beijing 100012, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
Recommended Citation
GB/T 7714
Teng Man,Jin Jing,Fu Qiang,et al. Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices[J]. CHINESE SCIENCE BULLETIN,2013,58(4-5):500-506.
APA Teng Man,Jin Jing,Fu Qiang,Cai YaQi,Chen JiPing,&Wei FuSheng.(2013).Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices.CHINESE SCIENCE BULLETIN,58(4-5),500-506.
MLA Teng Man,et al."Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices".CHINESE SCIENCE BULLETIN 58.4-5(2013):500-506.
Files in This Item:
There are no files associated with this item.
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Teng Man]'s Articles
[Jin Jing]'s Articles
[Fu Qiang]'s Articles
Baidu academic
Similar articles in Baidu academic
[Teng Man]'s Articles
[Jin Jing]'s Articles
[Fu Qiang]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Teng Man]'s Articles
[Jin Jing]'s Articles
[Fu Qiang]'s Articles
Terms of Use
No data!
Social Bookmark/Share
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.