中国科学院大连化学物理研究所机构知识库
Advanced  
DICP OpenIR  > 中国科学院大连化学物理研究所  > 期刊论文
题名: A new type of chemically bonded phase for reversed-phase HPLC
作者: Huang, XJ;  Wang, J;  Liu, XL;  Cong, R
刊名: ANALYTICAL SCIENCES
发表日期: 2003-10-01
卷: 19, 期:10, 页:1391-1394
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical
研究领域[WOS]: Chemistry
英文摘要: A new type of ether-bonded packing for reversed-phase HPLC (RP-HPLC) was synthesized by reacting 1-octanol with beta- (3.4-epoxycyclohexyl)ethyltrimethoxysilane, followed by coupling the product onto porous silica. The prepared packing was characterized by elemental analysis, solid-state C-13 NMR, and Fourier transform infrared (FT-IR) spectroscopy. Chromatographic evaluations were performed by using a mixture of organic compounds as the analyte and methanol-water as binary mobile phase. The influence of the composition of organic modifier on the retention behavior of basic compounds was studied. The hydrolytic stability of the packing between pH 2.5 - 7.5 was also investigated. The results showed that the new stationary phase has excellent chromatographic properties and good hydrolytic stability.
关键词[WOS]: STATIONARY-PHASE ;  COLUMN PACKING
语种: 英语
WOS记录号: WOS:000186144700009
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/138212
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

Files in This Item:

There are no files associated with this item.


作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China

Recommended Citation:
Huang, XJ,Wang, J,Liu, XL,et al. A new type of chemically bonded phase for reversed-phase HPLC[J]. ANALYTICAL SCIENCES,2003,19(10):1391-1394.
Service
 Recommend this item
 Sava as my favorate item
 Show this item's statistics
 Export Endnote File
Google Scholar
 Similar articles in Google Scholar
 [Huang, XJ]'s Articles
 [Wang, J]'s Articles
 [Liu, XL]'s Articles
CSDL cross search
 Similar articles in CSDL Cross Search
 [Huang, XJ]‘s Articles
 [Wang, J]‘s Articles
 [Liu, XL]‘s Articles
Related Copyright Policies
Null
Social Bookmarking
  Add to CiteULike  Add to Connotea  Add to Del.icio.us  Add to Digg  Add to Reddit 
所有评论 (0)
暂无评论
 
评注功能仅针对注册用户开放,请您登录
您对该条目有什么异议,请填写以下表单,管理员会尽快联系您。
内 容:
Email:  *
单位:
验证码:   刷新
您在IR的使用过程中有什么好的想法或者建议可以反馈给我们。
标 题:
 *
内 容:
Email:  *
验证码:   刷新

Items in IR are protected by copyright, with all rights reserved, unless otherwise indicated.

 

 

Valid XHTML 1.0!
Powered by CSpace