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题名: Synthesis and properties of (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol and its benzylhalostannyl derivatives
作者: Ren, YJ;  Jia, CY;  Zhao, YM;  Li, P;  Li, H;  Chen, HL
关键词: (Z)-1-[2-(tribenzylstannyl)vinyl]-1-cycloheptanol ;  synthesis ;  property
刊名: CHINESE JOURNAL OF ORGANIC CHEMISTRY
发表日期: 2003-04-01
卷: 23, 期:4, 页:372-374
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Organic
研究领域[WOS]: Chemistry
英文摘要: 1-Ethynyl-1-cycloheptanol reacted with tribenzylstannyl hydride ( C6H5CH2)(3)SnH generating, the corresponding (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol (1). The compound 1 obtained reacted with one or two equivalents of halogen (I-2, Br-2 or ICl) to form the associated (Z)-1-[2-(dibenzylhalostannyl) vinyl]-1-cycloheptanol or ( Z)-1-[ 2 (benzyldihalostannyl) vinyl]-1-cycloheptanol (2 similar to 7), respectively. The organotin hydroxide 8 was prepared by the reaction, of 3 with KOH. All compounds were characterized by elemental analysis, IR and H-1 NMR spectra, and the antitumor activity of compounds 1, 3, 4, 6 and 7 was determined. And it was found that they were potent antitumor agents, being effective against P388 cells in mice.
关键词[WOS]: COMPLEXES
语种: 英语
WOS记录号: WOS:000182184600010
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/138214
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Dalian Univ Technol, Dept Chem, Dalian 116024, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China

Recommended Citation:
Ren, YJ,Jia, CY,Zhao, YM,et al. Synthesis and properties of (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol and its benzylhalostannyl derivatives[J]. CHINESE JOURNAL OF ORGANIC CHEMISTRY,2003,23(4):372-374.
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