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Synthesis and properties of (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol and its benzylhalostannyl derivatives
Ren, YJ; Jia, CY; Zhao, YM; Li, P; Li, H; Chen, HL
关键词(z)-1-[2-(Tribenzylstannyl)Vinyl]-1-cycloheptanol Synthesis Property
刊名CHINESE JOURNAL OF ORGANIC CHEMISTRY
2003-04-01
23期:4页:372-374
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Organic
研究领域[WOS]Chemistry
关键词[WOS]COMPLEXES
英文摘要1-Ethynyl-1-cycloheptanol reacted with tribenzylstannyl hydride ( C6H5CH2)(3)SnH generating, the corresponding (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol (1). The compound 1 obtained reacted with one or two equivalents of halogen (I-2, Br-2 or ICl) to form the associated (Z)-1-[2-(dibenzylhalostannyl) vinyl]-1-cycloheptanol or ( Z)-1-[ 2 (benzyldihalostannyl) vinyl]-1-cycloheptanol (2 similar to 7), respectively. The organotin hydroxide 8 was prepared by the reaction, of 3 with KOH. All compounds were characterized by elemental analysis, IR and H-1 NMR spectra, and the antitumor activity of compounds 1, 3, 4, 6 and 7 was determined. And it was found that they were potent antitumor agents, being effective against P388 cells in mice.
语种英语
WOS记录号WOS:000182184600010
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/138214
专题中国科学院大连化学物理研究所
作者单位1.Dalian Univ Technol, Dept Chem, Dalian 116024, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
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GB/T 7714
Ren, YJ,Jia, CY,Zhao, YM,et al. Synthesis and properties of (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol and its benzylhalostannyl derivatives[J]. CHINESE JOURNAL OF ORGANIC CHEMISTRY,2003,23(4):372-374.
APA Ren, YJ,Jia, CY,Zhao, YM,Li, P,Li, H,&Chen, HL.(2003).Synthesis and properties of (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol and its benzylhalostannyl derivatives.CHINESE JOURNAL OF ORGANIC CHEMISTRY,23(4),372-374.
MLA Ren, YJ,et al."Synthesis and properties of (Z)-1-[2-(tribenzylstannyl) vinyl]-1-cycloheptanol and its benzylhalostannyl derivatives".CHINESE JOURNAL OF ORGANIC CHEMISTRY 23.4(2003):372-374.
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