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Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection
Chen, GF; You, JM; Zhang, YK
关键词2-(9-carbazole)-ethyl Chloroformate High Performance Liquid Chromatography Pre-column Derivatization Alcohols
刊名CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
2003
31期:1页:62-65
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]METHANOL ; ETHANOL
英文摘要A novel fluorescence and ultraviolet labelling reagent, 2-(9-carbazole)-ethyl chloroformate, has been utilized as pre-column derivatization reagent for 15 aliphatic alcohols. The optimal derivatization conditions were investigated,. The results indicate that the derivatizing temperature is at 80degreesC and reaction time is 15 min and pyridine is used as catalyst. high performance liquid chromatography coupled with fluorescence detector was studied as a means of separation and determination of alcohols. The derivative baseline resolution has been acuired by optimizing separation condition. The limit of detection is 13.3similar to93.5 nmol/L.
语种英语
WOS记录号WOS:000180964300016
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被引频次:2[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/138392
专题中国科学院大连化学物理研究所
作者单位Acad Sinica, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 116011, Peoples R China
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GB/T 7714
Chen, GF,You, JM,Zhang, YK. Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2003,31(1):62-65.
APA Chen, GF,You, JM,&Zhang, YK.(2003).Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,31(1),62-65.
MLA Chen, GF,et al."Novel fluorescence derivatization reagent for the determination of alcohol by high performance liquid chromatography and fluorescent detection".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 31.1(2003):62-65.
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