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Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry
Kong, LA; Yu, ZY; Zou, HF; Sun, NC; Wu, LH; Ni, JY
关键词High Performance Liquid Chromatography-mass Spectrometry Rhizoma Chuanxiong Quality Control Ferulic Acid Ligustilide
刊名CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
2004-11-01
32期:11页:1501-1504
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
英文摘要The main active ingredients, ferulic acid. and ligustilide in Chinese traditional medicine, Rhizoma Chuanxiong, were separated and identified by high performance liquid chromatography-mass sepctrum (HPLC-MS). The standard ligustilide was prepared with preparative scale HPLC and identified by HPLC-diode array detection, mass spectrometry, infrared spectroscopy. Four kinds of extractiting solvent and extraction time affecting on the extraction efficiency of ferulic acid and ligustilide in Rhizoma Chuanxiong were examined, and a quality control method was also developed based on the quantitative determination of ferulic acid and liguistilide in extracted solutions of Rhizoma Chuanxiong by water and ethanol. The amount of ferulic acid and ligustilide in Rhizoma Chuanxiong determined are as much as 0.15% ( W/W) and 0.82% (W/W).
语种英语
WOS记录号WOS:000225615700021
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/138450
专题中国科学院大连化学物理研究所
作者单位Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatograph Res & Anal Ctr, Dalian 116011, Peoples R China
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Kong, LA,Yu, ZY,Zou, HF,et al. Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2004,32(11):1501-1504.
APA Kong, LA,Yu, ZY,Zou, HF,Sun, NC,Wu, LH,&Ni, JY.(2004).Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,32(11),1501-1504.
MLA Kong, LA,et al."Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 32.11(2004):1501-1504.
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