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题名: Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry
作者: Kong, LA;  Yu, ZY;  Zou, HF;  Sun, NC;  Wu, LH;  Ni, JY
关键词: high performance liquid chromatography-mass spectrometry ;  Rhizoma Chuanxiong ;  quality control ;  ferulic acid ;  ligustilide
刊名: CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
发表日期: 2004-11-01
卷: 32, 期:11, 页:1501-1504
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical
研究领域[WOS]: Chemistry
英文摘要: The main active ingredients, ferulic acid. and ligustilide in Chinese traditional medicine, Rhizoma Chuanxiong, were separated and identified by high performance liquid chromatography-mass sepctrum (HPLC-MS). The standard ligustilide was prepared with preparative scale HPLC and identified by HPLC-diode array detection, mass spectrometry, infrared spectroscopy. Four kinds of extractiting solvent and extraction time affecting on the extraction efficiency of ferulic acid and ligustilide in Rhizoma Chuanxiong were examined, and a quality control method was also developed based on the quantitative determination of ferulic acid and liguistilide in extracted solutions of Rhizoma Chuanxiong by water and ethanol. The amount of ferulic acid and ligustilide in Rhizoma Chuanxiong determined are as much as 0.15% ( W/W) and 0.82% (W/W).
语种: 英语
WOS记录号: WOS:000225615700021
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/138450
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatograph Res & Anal Ctr, Dalian 116011, Peoples R China

Recommended Citation:
Kong, LA,Yu, ZY,Zou, HF,et al. Determination of the active ingredients in Rhizoma Chuanxiong by high performance liquid chromatography-mass spectrometry[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2004,32(11):1501-1504.
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