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Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column
Wang, JF; Meng, ZH; Zhou, LM; Wang, QH; Zhu, DQ
关键词High Performance Liquid Chromatography Column In Situ Polymerization (Methacrylic Acid-styrene-divinylbenzene) Copolymer Polycyclic Aromatic Hydrocarbons
刊名CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
1999-07-01
27期:7页:745-748
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]REVERSED-PHASE CHROMATOGRAPHY ; SEPARATION MEDIUM ; MACROPOROUS POLY(STYRENE-CO-DIVINYLBENZENE) ; MONOLITHIC ROD ; POLYMERS
英文摘要A novel high efficiency rod-shape poly(methacrylic acid-co-styrene-co-divinylbenzene) high performance liquid chromatographic column was prepared by a free-radical polymerization directly within the column. Scanning electron micrograph revealed the macropores of the copolymer column media. It had excellent permeability and the column pressure was only 2.5 MPa at a flow-rate of 2.0 mL/min with acetonitrile-water (90/10, V/V) as mobile phase. It also showed the rather high efficiency with the theoretical plates being 40,000 plates per meter. Aromatic acids and polycyclic aromatic hydrocarbons were separated within 4 and 10 minutes, respectively.
语种英语
WOS记录号WOS:000081672300001
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被引频次:1[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/138568
专题中国科学院大连化学物理研究所
作者单位Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China
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GB/T 7714
Wang, JF,Meng, ZH,Zhou, LM,et al. Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,1999,27(7):745-748.
APA Wang, JF,Meng, ZH,Zhou, LM,Wang, QH,&Zhu, DQ.(1999).Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,27(7),745-748.
MLA Wang, JF,et al."Preparation and evaluation of high efficient rod-shape poly(methacrylic acid-styrene-divinylbenzene) high performance liquid chromatographic column".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 27.7(1999):745-748.
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