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Synthesis and crystal structure of the derivative of beta-elemene C20H33N center dot Cl3CCOOH
Gong, GL; Cheng, GB; Hu, JH; Dai, JY; Wu, QJ
关键词Beta-elemene Derivative Crystal Structure Synthesis
刊名CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
1999
18期:4页:277-281
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Inorganic & Nuclear ; Crystallography
研究领域[WOS]Chemistry ; Crystallography
英文摘要The structure of the piperidine derivative of beta-elemene C20H33N . Cl3CCOOH was determined by X-ray crystallography. The crystal belongs to the orthorhombic system, space group P2(1)2(1)2(1), a=12.303(4), b=22.064(7), c=9.002 (4) Angstrom, V=2444(2) Angstrom(3), Z=4, M-r=450.88, D-c=1.23g/cm(3), mu(MoK alpha)=3.91cm(-1), F(000)=960, Final R=0.050, R-w=0.067 for 2393 reflections [I>3 sigma(I)], GOF=1.91. The title compound is composed of trichloroacetate and the elemenyl piperidine cation. The latter contains two hexacyclic rings of beta-elemene and piperidine, which adopt the chair conformations.
语种英语
WOS记录号WOS:000081538300009
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被引频次:1[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/138608
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Fujian Inst Res Struct Matter, Fuzhou 350002, Peoples R China
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GB/T 7714
Gong, GL,Cheng, GB,Hu, JH,et al. Synthesis and crystal structure of the derivative of beta-elemene C20H33N center dot Cl3CCOOH[J]. CHINESE JOURNAL OF STRUCTURAL CHEMISTRY,1999,18(4):277-281.
APA Gong, GL,Cheng, GB,Hu, JH,Dai, JY,&Wu, QJ.(1999).Synthesis and crystal structure of the derivative of beta-elemene C20H33N center dot Cl3CCOOH.CHINESE JOURNAL OF STRUCTURAL CHEMISTRY,18(4),277-281.
MLA Gong, GL,et al."Synthesis and crystal structure of the derivative of beta-elemene C20H33N center dot Cl3CCOOH".CHINESE JOURNAL OF STRUCTURAL CHEMISTRY 18.4(1999):277-281.
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