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题名: Synthesis and crystal structure of the derivative of beta-elemene C20H33N center dot Cl3CCOOH
作者: Gong, GL;  Cheng, GB;  Hu, JH;  Dai, JY;  Wu, QJ
关键词: beta-elemene derivative ;  crystal structure ;  synthesis
刊名: CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
发表日期: 1999
卷: 18, 期:4, 页:277-281
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Inorganic & Nuclear ;  Crystallography
研究领域[WOS]: Chemistry ;  Crystallography
英文摘要: The structure of the piperidine derivative of beta-elemene C20H33N . Cl3CCOOH was determined by X-ray crystallography. The crystal belongs to the orthorhombic system, space group P2(1)2(1)2(1), a=12.303(4), b=22.064(7), c=9.002 (4) Angstrom, V=2444(2) Angstrom(3), Z=4, M-r=450.88, D-c=1.23g/cm(3), mu(MoK alpha)=3.91cm(-1), F(000)=960, Final R=0.050, R-w=0.067 for 2393 reflections [I>3 sigma(I)], GOF=1.91. The title compound is composed of trichloroacetate and the elemenyl piperidine cation. The latter contains two hexacyclic rings of beta-elemene and piperidine, which adopt the chair conformations.
语种: 英语
WOS记录号: WOS:000081538300009
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/138608
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Fujian Inst Res Struct Matter, Fuzhou 350002, Peoples R China

Recommended Citation:
Gong, GL,Cheng, GB,Hu, JH,et al. Synthesis and crystal structure of the derivative of beta-elemene C20H33N center dot Cl3CCOOH[J]. CHINESE JOURNAL OF STRUCTURAL CHEMISTRY,1999,18(4):277-281.
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