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In situ NMR study of asymmetric borane reduction reaction - an abnormal factor in the temperature effect on the bis-oxazaborolidine catalyst and the relationship between the catalyst structure and selectivity
Zhao, JK; Bao, XH; Liu, XM; Wan, BS; Han, XW; Yang, CG; Hang, JF; Feng, Y; Jiang, B
刊名TETRAHEDRON-ASYMMETRY
2000-08-25
11期:16页:3351-3359
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Inorganic & Nuclear ; Chemistry, Organic ; Chemistry, Physical
研究领域[WOS]Chemistry
关键词[WOS]ENANTIOSELECTIVE REDUCTION ; PROCHIRAL KETONES ; ALCOHOLS
英文摘要The relationship between the structure of the catalyst and the selectivity in the asymmetric borane reduction reaction of prochiral ketones is discussed. The variation of the catalyst itself at low temperature is observed by the in situ NMR method and the origin of the temperature effect of the reaction is proposed. It is concluded that the amount of the effective component of the catalyst present has an important effect on the enantioselectivity. (C) 2000 Elsevier Science Ltd. All rights reserved.
语种英语
WOS记录号WOS:000089843700015
引用统计
被引频次:13[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/138729
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Shanghai Inst Organ Chem, Shanghai 200032, Peoples R China
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GB/T 7714
Zhao, JK,Bao, XH,Liu, XM,et al. In situ NMR study of asymmetric borane reduction reaction - an abnormal factor in the temperature effect on the bis-oxazaborolidine catalyst and the relationship between the catalyst structure and selectivity[J]. TETRAHEDRON-ASYMMETRY,2000,11(16):3351-3359.
APA Zhao, JK.,Bao, XH.,Liu, XM.,Wan, BS.,Han, XW.,...&Jiang, B.(2000).In situ NMR study of asymmetric borane reduction reaction - an abnormal factor in the temperature effect on the bis-oxazaborolidine catalyst and the relationship between the catalyst structure and selectivity.TETRAHEDRON-ASYMMETRY,11(16),3351-3359.
MLA Zhao, JK,et al."In situ NMR study of asymmetric borane reduction reaction - an abnormal factor in the temperature effect on the bis-oxazaborolidine catalyst and the relationship between the catalyst structure and selectivity".TETRAHEDRON-ASYMMETRY 11.16(2000):3351-3359.
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