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题名: Heat capacity and thermodynamic properties of (1R,2S,5R)-2-i-propyI-5-methylcyclohexyl diazoacetate
作者: Di, YY;  Tan, ZC;  Li, ZN;  Song, YJ;  Zheng, Y;  Meng, SH;  Qu, SS
关键词: (1R,2S,5R)-2-i-propyi-5-methylcyclohexyl diazoacetate ;  heat capacity ;  adiabatic calorimeter ;  chemical purity
刊名: THERMOCHIMICA ACTA
发表日期: 2000-11-13
卷: 362, 期:1-2, 页:7-12
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical ;  Chemistry, Physical
研究领域[WOS]: Chemistry
英文摘要: Heat capacities of (1R,2S,5R)-2-i-propyl-5-methylcyclohexyl diazoacetate have been measured with a small sample adiabatic calorimeter over the temperature range from 78 to 344 K. The melting point, molar enthalpy and entropy of fusion as well as the chemical purity of this compound were determined to be 320.419 +/- 0.017 K, 17.203 +/- 0.005 kJ mol(-1),53.689 +/- 0.013JK(-1) mol(-1) and 99.61 mol%, respectively, on the basis of the heat-capacity measurements. The extrapolated melting temperature for the absolutely pure compound obtained from fractional melting experiments was 320.602 K. (C) 2000 Elsevier Science B.V. All rights reserved.
语种: 英语
WOS记录号: WOS:000165324700002
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/138731
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Thermochem Lab, Dalian 116023, Peoples R China
2.Wuhan Univ, Coll Chem & Environm Sci, Wuhan 430072, Peoples R China

Recommended Citation:
Di, YY,Tan, ZC,Li, ZN,et al. Heat capacity and thermodynamic properties of (1R,2S,5R)-2-i-propyI-5-methylcyclohexyl diazoacetate[J]. THERMOCHIMICA ACTA,2000,362(1-2):7-12.
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