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题名: Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography
作者: Huang, XJ;  Wang, JD;  Liu, XL;  Cong, RZ
关键词: high performance liquid chromatography ;  double-amine stationary phase ;  reversed phase packing
刊名: CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
发表日期: 2002-09-01
卷: 30, 期:9, 页:1048-1052
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical
研究领域[WOS]: Chemistry
英文摘要: A novel double-amine packing (DABP) for reversed-phase high performance liquid chromatography (RP-HPLC) was synthesized by the reaction of hexyldiamine with beta-(3,4-epoxycyclohexyl) ethyltrimethoxy silane, the intermediate product was coupled onto porous silica to get the intermediate product II, then the product II was reacted with octanoyl chloride under catalytst. Characterization of the prepared packing was carried out with elemental analysis, solid-state C-13 nuclear magnetic resonance and Fourier transform infrared (FF-IR). The chromatographic evaluation was carried out by using organic components including acidic, basic and neutral analytes as probe molecules. The results show that the separate mechanism of basic analytes on the DABP include shydrophobicity and ion repulse.
语种: 英语
WOS记录号: WOS:000178379800006
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/139207
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China

Recommended Citation:
Huang, XJ,Wang, JD,Liu, XL,et al. Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2002,30(9):1048-1052.
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