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Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography
Huang, XJ; Wang, JD; Liu, XL; Cong, RZ
关键词High Performance Liquid Chromatography Double-amine Stationary Phase Reversed Phase Packing
刊名CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
2002-09-01
30期:9页:1048-1052
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
英文摘要A novel double-amine packing (DABP) for reversed-phase high performance liquid chromatography (RP-HPLC) was synthesized by the reaction of hexyldiamine with beta-(3,4-epoxycyclohexyl) ethyltrimethoxy silane, the intermediate product was coupled onto porous silica to get the intermediate product II, then the product II was reacted with octanoyl chloride under catalytst. Characterization of the prepared packing was carried out with elemental analysis, solid-state C-13 nuclear magnetic resonance and Fourier transform infrared (FF-IR). The chromatographic evaluation was carried out by using organic components including acidic, basic and neutral analytes as probe molecules. The results show that the separate mechanism of basic analytes on the DABP include shydrophobicity and ion repulse.
语种英语
WOS记录号WOS:000178379800006
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被引频次:1[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/139207
专题中国科学院大连化学物理研究所
作者单位Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China
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GB/T 7714
Huang, XJ,Wang, JD,Liu, XL,et al. Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2002,30(9):1048-1052.
APA Huang, XJ,Wang, JD,Liu, XL,&Cong, RZ.(2002).Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,30(9),1048-1052.
MLA Huang, XJ,et al."Synthesis, characterization and evaluation of a novel double-amine packing for reversed-phage high performance liquid chromatography".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 30.9(2002):1048-1052.
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