DICP OpenIR
Determination of Amines by high performance liquid chromatography with a pre-column derivatization and fluorescence detection
Zhang, L; Ping, GC; You, JM; Ming, YF; Zhang, WB; Zhang, YK
关键词Chloroformate Fluorescence Reagent Fluorescence Derivatization High Performance Liquid Chromatography Amines
刊名CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
2003-07-01
31期:7页:808-811
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]6-AMINOQUINOLYL-N-HYDROXYSUCCINIMIDYL CARBAMATE ; ACIDS
英文摘要2-(9-Carbazole) ethyl chloroformate (CEOC), a novel fluorescence derivatization reagent, has been firstly developed for the determiantion of amines. In a one-step procedure, CEOC reacts with the amines to form stable derivatives. Maximum yield is observed with a molar reagent excess of approximately 3 to 4 times for each of the amines. The method in conjunction with a gradient elution offers a baseline separation on a reversed-phase Hypersil BDS C-18 column. Mobile phase: A = acetonitrile/water (20/80, V/V); B = acetonitrile/water (95/5, V/V) flow rate = 1.0 mL/min; column temperature was set at 35 degreesC. The fluorescent derivatives are detected at lambda(ex)/lambda(em) = 293/365 nm. It was proved that CEOC-high performance liquid chromatography (HPLC) not only had excellent precision and accuracy but also high tolerance of the matrix of samples (including salt), therefore the method is suitable for the determination of biological materials, foods and feeds.
语种英语
WOS记录号WOS:000184609900009
引用统计
被引频次:2[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/139252
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116011, Peoples R China
2.Qufu Normal Univ, Dept Chem, Qufu 273165, Peoples R China
推荐引用方式
GB/T 7714
Zhang, L,Ping, GC,You, JM,et al. Determination of Amines by high performance liquid chromatography with a pre-column derivatization and fluorescence detection[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2003,31(7):808-811.
APA Zhang, L,Ping, GC,You, JM,Ming, YF,Zhang, WB,&Zhang, YK.(2003).Determination of Amines by high performance liquid chromatography with a pre-column derivatization and fluorescence detection.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,31(7),808-811.
MLA Zhang, L,et al."Determination of Amines by high performance liquid chromatography with a pre-column derivatization and fluorescence detection".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 31.7(2003):808-811.
条目包含的文件
条目无相关文件。
个性服务
推荐该条目
保存到收藏夹
查看访问统计
导出为Endnote文件
谷歌学术
谷歌学术中相似的文章
[Zhang, L]的文章
[Ping, GC]的文章
[You, JM]的文章
百度学术
百度学术中相似的文章
[Zhang, L]的文章
[Ping, GC]的文章
[You, JM]的文章
必应学术
必应学术中相似的文章
[Zhang, L]的文章
[Ping, GC]的文章
[You, JM]的文章
相关权益政策
暂无数据
收藏/分享
所有评论 (0)
暂无评论
 

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。