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THE H-1, C-13 NMR STUDIES ON ALKALOID PLATINUM(II) COMPLEXES
Yang Zhenyun; Han Xiuwen; Hu Jiehan; Chen Huilin
Source PublicationACTA PHYSICO-CHIMICA SINICA
1988
DOI10.3866/PKU.WHXB19880107
Volume4Issue:1Pages:32-36
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences
WOS SubjectChemistry, Physical
WOS Research AreaChemistry
AbstractThe C-13 and H-1 NMR spectra of antitumor alkaloid platinum complexes such as caffeine, theophylline and theobromine platinum (II)complexes were recorded. The H-1, C-13 chemical shifts and carbon hydrogen coupling conatants were obtained for these alkaloids and their platinum complexes. Compating the variations of 61, and 8c in, the Uganda before, and after coordination and combining with the determination of carbon platinum and hydrogen platinum coupling constants, we find that the alkaloids coordinate to platinum unidentately the coordination site is the double bond nitrogen atom on the five membered imidazole ring, The pla tinum (II) is coordinated with three chloride anions and one alkaloid ligand to form a mononuclear complex anion (PtLCl3)(-). By heterortuclear proton selected decoupling technique, all the H-1 and C-13 NUR spectral linen were assigned.
Language英语
WOS IDWOS:000207571200007
Citation statistics
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/139406
Collection中国科学院大连化学物理研究所
AffiliationAcad Sinica, Dalian Inst Chem Phys, Dalian, Peoples R China
Recommended Citation
GB/T 7714
Yang Zhenyun,Han Xiuwen,Hu Jiehan,et al. THE H-1, C-13 NMR STUDIES ON ALKALOID PLATINUM(II) COMPLEXES[J]. ACTA PHYSICO-CHIMICA SINICA,1988,4(1):32-36.
APA Yang Zhenyun,Han Xiuwen,Hu Jiehan,&Chen Huilin.(1988).THE H-1, C-13 NMR STUDIES ON ALKALOID PLATINUM(II) COMPLEXES.ACTA PHYSICO-CHIMICA SINICA,4(1),32-36.
MLA Yang Zhenyun,et al."THE H-1, C-13 NMR STUDIES ON ALKALOID PLATINUM(II) COMPLEXES".ACTA PHYSICO-CHIMICA SINICA 4.1(1988):32-36.
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