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题名: THE H-1, C-13 NMR STUDIES ON ALKALOID PLATINUM(II) COMPLEXES
作者: Yang Zhenyun1;  Han Xiuwen1;  Hu Jiehan1;  Chen Huilin1
刊名: ACTA PHYSICO-CHIMICA SINICA
发表日期: 1988
DOI: 10.3866/PKU.WHXB19880107
卷: 4, 期:1, 页:32-36
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Physical
研究领域[WOS]: Chemistry
英文摘要: The C-13 and H-1 NMR spectra of antitumor alkaloid platinum complexes such as caffeine, theophylline and theobromine platinum (II)complexes were recorded. The H-1, C-13 chemical shifts and carbon hydrogen coupling conatants were obtained for these alkaloids and their platinum complexes. Compating the variations of 61, and 8c in, the Uganda before, and after coordination and combining with the determination of carbon platinum and hydrogen platinum coupling constants, we find that the alkaloids coordinate to platinum unidentately the coordination site is the double bond nitrogen atom on the five membered imidazole ring, The pla tinum (II) is coordinated with three chloride anions and one alkaloid ligand to form a mononuclear complex anion (PtLCl3)(-). By heterortuclear proton selected decoupling technique, all the H-1 and C-13 NUR spectral linen were assigned.
语种: 英语
WOS记录号: WOS:000207571200007
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/139406
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Acad Sinica, Dalian Inst Chem Phys, Dalian, Peoples R China

Recommended Citation:
Yang Zhenyun,Han Xiuwen,Hu Jiehan,et al. THE H-1, C-13 NMR STUDIES ON ALKALOID PLATINUM(II) COMPLEXES[J]. ACTA PHYSICO-CHIMICA SINICA,1988,4(1):32-36.
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