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题名: Low-temperature heat capacity and thermal decomposition of crystalline [Er-2(His center dot H+)(H2O)8](ClO4)(6)center dot 4H(2)O
作者: Lan, XX;  Tan, ZC;  Liu, BP;  Nan, ZD;  Sun, LX;  Xu, F
关键词: adiabatic calorimeter ;  heat capacity ;  histidine rare earth complex ;  TG analysis ;  thermal decomposition
刊名: THERMOCHIMICA ACTA
发表日期: 2004-06-23
DOI: 10.1016/j.tca.2003.11.032
卷: 416, 期:1-2, 页:55-58
收录类别: ISTP ;  SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical ;  Chemistry, Physical
研究领域[WOS]: Chemistry
英文摘要: The heat capacities of rare earth complex with amino acid histidine, [Er-2(His.H+)(H2O)(8)](ClO4)(6).4H(2)O, were measured with an automatic adiabatic calorimeter from 79 to 320 K. It was found that there was a sudden increment in heat capacity within the temperature range 182-190 K. Thermal decomposition behavior of the complex in nitrogen atmosphere was studied by thermogravimetric (TG) analysis, and a possible decomposition mechanism was suggested according to TG-DTG results. (C) 2003 Elsevier B.V. All rights reserved.
语种: 英语
WOS记录号: WOS:000222154700013
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/139528
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Thermochem Lab, Dalian 116023, Peoples R China

Recommended Citation:
Lan, XX,Tan, ZC,Liu, BP,et al. Low-temperature heat capacity and thermal decomposition of crystalline [Er-2(His center dot H+)(H2O)8](ClO4)(6)center dot 4H(2)O[J]. THERMOCHIMICA ACTA,2004,416(1-2):55-58.
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