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A facile preparation of uronates via selective oxidation with TEMPO/KBr/Ca(OCl)(2) under aqueous conditions
Feng, L; Peng, WJ; Xu, W; Han, XW; Yu, B
关键词Uronate Oxidation Tempo Ca(Ocl)(2) Saponin
刊名CARBOHYDRATE RESEARCH
2004-04-28
DOI10.1016/j.carres.2004.02.001
339期:6页:1219-1223
收录类别SCI ; IC
文章类型Article
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
类目[WOS]Biochemistry & Molecular Biology ; Chemistry, Applied ; Chemistry, Organic
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]TEMPO-MEDIATED OXIDATION ; STREPTOCOCCUS-PNEUMONIAE TYPE-3 ; CAPSULAR POLYSACCHARIDE ; SECONDARY ALCOHOLS ; 2-PHASE CONDITIONS ; OXOAMMONIUM SALTS ; HYDROGEN-PEROXIDE ; CARBOXYLIC-ACIDS ; TRISACCHARIDES ; GLUCURONIDES
英文摘要Addition of solid Ca(OCI)(2) as the terminal oxidant in the TEMPO-mediated selective oxidation has the benefit of easier operation. A variety of partially protected saccharide derivatives (1a-1) have been successfully converted into the corresponding uronate derivatives. including disaccharide building blocks for GAG fragments and precursors to saponins. The beneficial effect of Aliquat 336 was also disclosed in the oxidation of certain substrates. (C) 2004 Elsevier Ltd. All rights reserved.
语种英语
WOS记录号WOS:000220934200028
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被引频次:27[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/139546
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Shanghai Inst Organ Chem, State Key Lab Bioorgan & Nat Prod Chem, Shanghai 200032, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalyst, Dalian 116023, Peoples R China
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GB/T 7714
Feng, L,Peng, WJ,Xu, W,et al. A facile preparation of uronates via selective oxidation with TEMPO/KBr/Ca(OCl)(2) under aqueous conditions[J]. CARBOHYDRATE RESEARCH,2004,339(6):1219-1223.
APA Feng, L,Peng, WJ,Xu, W,Han, XW,&Yu, B.(2004).A facile preparation of uronates via selective oxidation with TEMPO/KBr/Ca(OCl)(2) under aqueous conditions.CARBOHYDRATE RESEARCH,339(6),1219-1223.
MLA Feng, L,et al."A facile preparation of uronates via selective oxidation with TEMPO/KBr/Ca(OCl)(2) under aqueous conditions".CARBOHYDRATE RESEARCH 339.6(2004):1219-1223.
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