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Molar heat capacity and thermodynamic properties of 4-methyl-4-cyclohexene-1,2-dicarboxylic anhydride [C9H10O3]
Lv, XC; Tan, ZC; Shi, Q; Zhang, HT; Sun, LX; Zhang, T
刊名JOURNAL OF CHEMICAL AND ENGINEERING DATA
2005-05-01
DOI10.1021/je049585t
50期:3页:932-935
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences ; Technology
类目[WOS]Chemistry, Multidisciplinary ; Engineering, Chemical
研究领域[WOS]Chemistry ; Engineering
关键词[WOS]CALORIMETER
英文摘要The molar heat capacity C-p,C-m of 4-methyl-4-cyclohexene-1,2-dicarboxylic anhydride was measured over the temperature range from T = 80 K to T = 361 K with a small-sample automated adiabatic calorimeter. The melting point T-m and the molar enthalpy &UDelta;H-fus(m) and entropy &UDelta;S-fus(m) of fusion for the compound were determined to be (335.54 ± 0.41) K, (17.67 ± 0.04) kJ• mol(-1), and (52.65 ± 0.04) J• K-1• mol(-1), respectively. Thermodynamic functions [H-T - H-298.15] and [S-T - S-298.15] were derived in the temperature range from T = 80 K to T = 361 K with a temperature interval of 5 K. The purity of the sample in mole fraction used in the adiabatic calorimetry study was determined to be 0.9940 by using the fractional melting technique. The thermal stability of the compound was investigated by differential scanning calorimetry (DSC) and a thermogravimetric (TG) technique, and the process of the mass loss of the sample was due to evaporation instead of thermal decomposition.
语种英语
WOS记录号WOS:000229128300032
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/139802
专题中国科学院大连化学物理研究所
作者单位Chinese Acad Sci, Dalian Inst Chem Phys, Thermochem Lab, Dalian 116023, Peoples R China
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GB/T 7714
Lv, XC,Tan, ZC,Shi, Q,et al. Molar heat capacity and thermodynamic properties of 4-methyl-4-cyclohexene-1,2-dicarboxylic anhydride [C9H10O3][J]. JOURNAL OF CHEMICAL AND ENGINEERING DATA,2005,50(3):932-935.
APA Lv, XC,Tan, ZC,Shi, Q,Zhang, HT,Sun, LX,&Zhang, T.(2005).Molar heat capacity and thermodynamic properties of 4-methyl-4-cyclohexene-1,2-dicarboxylic anhydride [C9H10O3].JOURNAL OF CHEMICAL AND ENGINEERING DATA,50(3),932-935.
MLA Lv, XC,et al."Molar heat capacity and thermodynamic properties of 4-methyl-4-cyclohexene-1,2-dicarboxylic anhydride [C9H10O3]".JOURNAL OF CHEMICAL AND ENGINEERING DATA 50.3(2005):932-935.
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