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Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry
Zhang, Jie; Tao, Dingyin; Duan, Jicheng; Liang, Zhen; Zhang, Weibing; Zhang, Lihua; Huo, Yushu; Zhang, Yukui
关键词Comprehensive Two-dimensional Liquid Chromatography Traditional Chinese Medicine Adinandra Nitida Mass Spectrometer Monolithic Column
刊名ANALYTICAL AND BIOANALYTICAL CHEMISTRY
2006-10-01
DOI10.1007/s00216-006-0539-6
386期:3页:586-593
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]TRADITIONAL CHINESE MEDICINES ; MULTIDIMENSIONAL SEPARATION ; STATIONARY PHASES ; PERFORMANCE ; COLUMN ; RESOLUTION ; DISCOVERY ; MIXTURES ; PROTEINS
英文摘要A comprehensive two-dimensional liquid chromatographic (2D-LC) separation system based on the combination of a CN column and a Merck Chromolith Flash reversed-phase column was developed for the separation of components in Adinandra nitida, one type of traditional Chinese medicine (TCM). The two dimensions were connected by a ten-port, dual-position valve controlled automatically by software written in-house. The effluents were detected by both ultraviolet and atmospheric pressure chemical ionization source ion trap tandem mass spectrometry (MS). The calculated peak capacity of the 2D-LC-MS/MS system was above 1240. More than 57 components were resolved in the methanol extract from Adinandra nitida leaves, and five of these were identified based on their relative retention times, molecular weights and MS/MS spectra.
语种英语
WOS记录号WOS:000240713500020
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/139990
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatogr Res & Anal Ctr, Dalian 116023, Peoples R China
2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78229 USA
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GB/T 7714
Zhang, Jie,Tao, Dingyin,Duan, Jicheng,et al. Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry[J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY,2006,386(3):586-593.
APA Zhang, Jie.,Tao, Dingyin.,Duan, Jicheng.,Liang, Zhen.,Zhang, Weibing.,...&Zhang, Yukui.(2006).Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry.ANALYTICAL AND BIOANALYTICAL CHEMISTRY,386(3),586-593.
MLA Zhang, Jie,et al."Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry".ANALYTICAL AND BIOANALYTICAL CHEMISTRY 386.3(2006):586-593.
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