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Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry
Zhang, Jie; Tao, Dingyin; Duan, Jicheng; Liang, Zhen; Zhang, Weibing; Zhang, Lihua; Huo, Yushu; Zhang, Yukui
KeywordComprehensive Two-dimensional Liquid Chromatography Traditional Chinese Medicine Adinandra Nitida Mass Spectrometer Monolithic Column
Source PublicationANALYTICAL AND BIOANALYTICAL CHEMISTRY
2006-10-01
DOI10.1007/s00216-006-0539-6
Volume386Issue:3Pages:586-593
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Life Sciences & Biomedicine ; Physical Sciences
WOS SubjectBiochemical Research Methods ; Chemistry, Analytical
WOS Research AreaBiochemistry & Molecular Biology ; Chemistry
WOS KeywordTRADITIONAL CHINESE MEDICINES ; MULTIDIMENSIONAL SEPARATION ; STATIONARY PHASES ; PERFORMANCE ; COLUMN ; RESOLUTION ; DISCOVERY ; MIXTURES ; PROTEINS
AbstractA comprehensive two-dimensional liquid chromatographic (2D-LC) separation system based on the combination of a CN column and a Merck Chromolith Flash reversed-phase column was developed for the separation of components in Adinandra nitida, one type of traditional Chinese medicine (TCM). The two dimensions were connected by a ten-port, dual-position valve controlled automatically by software written in-house. The effluents were detected by both ultraviolet and atmospheric pressure chemical ionization source ion trap tandem mass spectrometry (MS). The calculated peak capacity of the 2D-LC-MS/MS system was above 1240. More than 57 components were resolved in the methanol extract from Adinandra nitida leaves, and five of these were identified based on their relative retention times, molecular weights and MS/MS spectra.
Language英语
WOS IDWOS:000240713500020
Citation statistics
Cited Times:28[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/139990
Collection中国科学院大连化学物理研究所
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatogr Res & Anal Ctr, Dalian 116023, Peoples R China
2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78229 USA
Recommended Citation
GB/T 7714
Zhang, Jie,Tao, Dingyin,Duan, Jicheng,et al. Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry[J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY,2006,386(3):586-593.
APA Zhang, Jie.,Tao, Dingyin.,Duan, Jicheng.,Liang, Zhen.,Zhang, Weibing.,...&Zhang, Yukui.(2006).Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry.ANALYTICAL AND BIOANALYTICAL CHEMISTRY,386(3),586-593.
MLA Zhang, Jie,et al."Separation and identification of compounds in Adinandra nitida by comprehensive two-dimensional liquid chromatography coupled to atmospheric pressure chemical ionization source ion trap tandem mass spectrometry".ANALYTICAL AND BIOANALYTICAL CHEMISTRY 386.3(2006):586-593.
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