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题名: Synthesis and thermodynamic properties of a metal-organic framework: [LaCu6(mu-OH)(3)(Gly)(6)im(6)](ClO4)(6)
作者: Lv, Xue-Chuan;  Tan, Zhi-Cheng;  Gao, Xiao-Han;  Zhang, Zhi-Heng;  Yang, Li-Ni;  Zhao, Jun-Ning;  Sun, Li-Xian;  Zhang, Tao
关键词: [LaCu6(mu-OH)(3)(Gly)(6)im(6)](ClO4)(6) ;  metal-organic frameworks ;  adiabatic calorimetry ;  heat capacity ;  thermal analysis
刊名: THERMOCHIMICA ACTA
发表日期: 2006-11-15
DOI: 10.1016/j.tca.2006.07.025
卷: 450, 期:1-2, 页:102-104
收录类别: ISTP ;  SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical ;  Chemistry, Physical
研究领域[WOS]: Chemistry
英文摘要: A metal-organic complex, which has the potential property of absorbing gases, [LaCu6(mu-OH)(3)(Gly)(6)im(6)](ClO4)(6) was synthesized through the self-assembly of La3+, Cu2+, glycine (Gly) and imidazole (Im) in aqueous solution and characterized by IR, element analysis and powder XRD. The molar heat capacity, C-p,C-m, was measured from T = 80 to 390 K with an automated adiabatic calorimeter. The thermodynamic functions [H-T - H-298.15] and [S-T - S298.15] were derived from the heat capacity data with temperature interval of 5 K. The thermal stability of the complex was investigated by differential scanning calorimetry (DSC). (c) 2006 Elsevier B.V. All rights reserved.
关键词[WOS]: HEAT-CAPACITIES ;  ADIABATIC CALORIMETER
语种: 英语
WOS记录号: WOS:000242290300021
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/140075
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Thermochem Lab, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China

Recommended Citation:
Lv, Xue-Chuan,Tan, Zhi-Cheng,Gao, Xiao-Han,et al. Synthesis and thermodynamic properties of a metal-organic framework: [LaCu6(mu-OH)(3)(Gly)(6)im(6)](ClO4)(6)[J]. THERMOCHIMICA ACTA,2006,450(1-2):102-104.
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