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题名: Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent
作者: Qu Qishu;  Tang Xiaoqing;  Wang Chengyin;  Yang Gongjun;  Hu Xiaoya;  Zhang Yukui;  Yan Chao
关键词: capillary electrophoresis ;  D-amino acid ;  derivatization
刊名: CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
发表日期: 2006-11-01
卷: 34, 期:11, 页:1587-1590
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical
研究领域[WOS]: Chemistry
英文摘要: A new method for the separation of 19 standard D-amino acids and glycine ( Gly) by capillary electrophoresis ( CE) using p-acetamidobenzenesulfonyl fluoride ( PAABS-F) as precolumn derivatization reagent has been developed. The separation conditions were carefully studied and optimized. The experimental results showed that 20 mmmol/L sodium borate ( pH 9.3), 126 mmmol/L sodium dodecyl sulfate, 8 mmol/L,8-cyclodextrin and 20 mmol/L NaCl were the optimal conditions for the CE separation. Under the optimal conditions, 19 stangdard D-amino acids and Gly were successfully achied with baseline separation within 16 min by CE.
关键词[WOS]: CHROMATOGRAPHY
语种: 英语
WOS记录号: WOS:000244672100016
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/140251
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Yangzhou Univ, Jiangsu Key Lab Environm Mat & Environm Engn, Coll Chem & Chem Engn, Yangzhou 225002, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 116011, Peoples R China

Recommended Citation:
Qu Qishu,Tang Xiaoqing,Wang Chengyin,et al. Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2006,34(11):1587-1590.
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