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题名: Multi-segment linear gradient optimization strategy based on resolution map in HPLC
作者: Shan Yichu;  Zhang Weibing;  Seidel-Morgenstern, Andreas;  Zhao Ruihuan;  Zhang Yukui
关键词: optimization ;  multi-segment ;  linear gradient ;  resolution map ;  liquid chromatography
刊名: SCIENCE IN CHINA SERIES B-CHEMISTRY
发表日期: 2006-08-01
DOI: 10.1007/s11426-006-2004-y
卷: 49, 期:4, 页:315-325
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Multidisciplinary
研究领域[WOS]: Chemistry
英文摘要: Based on the mechanism of chromatographic retention (the relationship between the retention of solute and the mobile phase conditions) and method of resolution map, several methods of optimizing multi-segment linear gradient elution conditions were proposed according to the different separation requirements of various samples. These methods were verified using literature data. Moreover, the advantages and disadvantages of these methods were compared. It was proved that the third method is a fast optimization method which is capable of separating all the components with relatively high resolution.
关键词[WOS]: PERFORMANCE LIQUID-CHROMATOGRAPHY ;  COMPUTER-AIDED OPTIMIZATION ;  ASSISTED RETENTION PREDICTION ;  THIN-LAYER-CHROMATOGRAPHY ;  COMPLEX SAMPLES ;  OPTIMIZING TEMPERATURE ;  EXCHANGE CHROMATOGRAPHY ;  EXPERIMENTAL-DESIGN ;  MOBILE-PHASE ;  SEPARATION
语种: 英语
WOS记录号: WOS:000240332800004
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/140301
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Max Planck Inst Dynam Komplexer, Tech Syst, D-39106 Magdeburg, Germany
2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116011, Peoples R China

Recommended Citation:
Shan Yichu,Zhang Weibing,Seidel-Morgenstern, Andreas,et al. Multi-segment linear gradient optimization strategy based on resolution map in HPLC[J]. SCIENCE IN CHINA SERIES B-CHEMISTRY,2006,49(4):315-325.
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