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Convenient preparation of chiral alpha,beta-epoxy ketones via Claisen-Schmidt condensation-epoxidation sequence
Wang, Yongcan; Ye, Jinxing; Liang, Xinmiao
KeywordAldehydes Asymmetric Catalysis Condensation Epoxidation Ketones One-pot
Source PublicationADVANCED SYNTHESIS & CATALYSIS
2007-05-01
DOI10.1002/adsc.200600592
Volume349Issue:7Pages:1033-1036
Indexed BySCI ; CCR
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences
WOS SubjectChemistry, Applied ; Chemistry, Organic
WOS Research AreaChemistry
WOS KeywordCATALYTIC ASYMMETRIC EPOXIDATION ; HIGHLY ENANTIOSELECTIVE EPOXIDATION ; TRANSFER MEDIATED EPOXIDATION ; PHASE-TRANSFER CATALYSTS ; ALPHA,BETA-UNSATURATED KETONES ; TRICHLOROISOCYANURIC ACID ; CINCHONA ALKALOIDS ; ENONES ; WATER
AbstractA novel Clasisen-Schmidt condensation-epoxidation sequence of aldehydes and ketones was developed to produce a series of chiral ap-epoxy ketones under asymmetric phase-transfer catalytic conditions. The organocatalytic method reported here can afford chiral alpha,beta-epoxy ketones under mild conditions with moderate to good yields and up to 96% ee.
Language英语
WOS IDWOS:000246990200006
Citation statistics
Cited Times:28[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/140394
Collection中国科学院大连化学物理研究所
Affiliation1.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
Recommended Citation
GB/T 7714
Wang, Yongcan,Ye, Jinxing,Liang, Xinmiao. Convenient preparation of chiral alpha,beta-epoxy ketones via Claisen-Schmidt condensation-epoxidation sequence[J]. ADVANCED SYNTHESIS & CATALYSIS,2007,349(7):1033-1036.
APA Wang, Yongcan,Ye, Jinxing,&Liang, Xinmiao.(2007).Convenient preparation of chiral alpha,beta-epoxy ketones via Claisen-Schmidt condensation-epoxidation sequence.ADVANCED SYNTHESIS & CATALYSIS,349(7),1033-1036.
MLA Wang, Yongcan,et al."Convenient preparation of chiral alpha,beta-epoxy ketones via Claisen-Schmidt condensation-epoxidation sequence".ADVANCED SYNTHESIS & CATALYSIS 349.7(2007):1033-1036.
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