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Synthesis, crystal structure and thermochemical study of [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5)
Lu Ji-Lin; Liu Bei-Ping; Tan Zhi-Cheng; Zhang Da-Shun; Li Lin; Chen Yuan-Dao; Shi Quan
关键词Gadolinium Perchlorate Glycine Complex Crystal Structure Standard Molar Enthalpy Of Formation
刊名ACTA CHIMICA SINICA
2007-10-28
65期:20页:2349-2355
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Multidisciplinary
研究领域[WOS]Chemistry
英文摘要The complex [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5) was synthesized by a microwave technology characterized by IR spectra and a TG-DTG technique. The crystal structure of the complex was determined by an X-ray diffraction method. The crystal is a ID chain structure, which belongs to a triclinic system with space group P (1) over bar, and cell parameters: a = 1.1569(17) nm, b = 1.4138(2) nm, c = 1.5642(2) nm, alpha = 96.910(2)degrees, beta = 102.735(2)degrees, gamma = 105.512(2)degrees, V = 2.3606(6) nm(3), Z = 2, and D-c = 2.144 g.cm(-3). By isoperibol solution-reaction calorimetry, the standard molar enthalpy of formation of the complex was determined to be -(7960.73 +/- 3.23)kJ.mol(-1).
语种英语
WOS记录号WOS:000250735300025
引用统计
被引频次:3[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/140432
专题中国科学院大连化学物理研究所
作者单位1.Hunan Univ Arts & Sci, Dept Chem & Chem Engn, Changde 415000, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
推荐引用方式
GB/T 7714
Lu Ji-Lin,Liu Bei-Ping,Tan Zhi-Cheng,et al. Synthesis, crystal structure and thermochemical study of [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5)[J]. ACTA CHIMICA SINICA,2007,65(20):2349-2355.
APA Lu Ji-Lin.,Liu Bei-Ping.,Tan Zhi-Cheng.,Zhang Da-Shun.,Li Lin.,...&Shi Quan.(2007).Synthesis, crystal structure and thermochemical study of [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5).ACTA CHIMICA SINICA,65(20),2349-2355.
MLA Lu Ji-Lin,et al."Synthesis, crystal structure and thermochemical study of [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5)".ACTA CHIMICA SINICA 65.20(2007):2349-2355.
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