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题名: Synthesis, crystal structure and thermochemical study of [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5)
作者: Lu Ji-Lin;  Liu Bei-Ping;  Tan Zhi-Cheng;  Zhang Da-Shun;  Li Lin;  Chen Yuan-Dao;  Shi Quan
关键词: gadolinium perchlorate ;  glycine ;  complex ;  crystal structure ;  standard molar enthalpy of formation
刊名: ACTA CHIMICA SINICA
发表日期: 2007-10-28
卷: 65, 期:20, 页:2349-2355
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Multidisciplinary
研究领域[WOS]: Chemistry
英文摘要: The complex [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5) was synthesized by a microwave technology characterized by IR spectra and a TG-DTG technique. The crystal structure of the complex was determined by an X-ray diffraction method. The crystal is a ID chain structure, which belongs to a triclinic system with space group P (1) over bar, and cell parameters: a = 1.1569(17) nm, b = 1.4138(2) nm, c = 1.5642(2) nm, alpha = 96.910(2)degrees, beta = 102.735(2)degrees, gamma = 105.512(2)degrees, V = 2.3606(6) nm(3), Z = 2, and D-c = 2.144 g.cm(-3). By isoperibol solution-reaction calorimetry, the standard molar enthalpy of formation of the complex was determined to be -(7960.73 +/- 3.23)kJ.mol(-1).
语种: 英语
WOS记录号: WOS:000250735300025
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/140432
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Hunan Univ Arts & Sci, Dept Chem & Chem Engn, Changde 415000, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China

Recommended Citation:
Lu Ji-Lin,Liu Bei-Ping,Tan Zhi-Cheng,et al. Synthesis, crystal structure and thermochemical study of [Gd-2(Gly)(6)(H2O)(4)](ClO4)(6)(H2O)(5)[J]. ACTA CHIMICA SINICA,2007,65(20):2349-2355.
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