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题名: Synthesis of a new intermediate for bioactive Lamellarins
作者: He, Yu-Rong;  You, Ye-Cheng;  Hu, Jie-Han;  Wang, Ai-Ling;  Yu, Xiao-Song;  Hu, Dai-Hua
刊名: BIOMEDICAL MATERIALS
发表日期: 2007-06-01
DOI: 10.1088/1748-6041/2/2/007
卷: 2, 期:2, 页:102-106
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Technology
类目[WOS]: Engineering, Biomedical ;  Materials Science, Biomaterials
研究领域[WOS]: Engineering ;  Materials Science
英文摘要: This paper reports two methods of synthesis for 1,2,4-trimethoxy-5-(1-methyl-2-phenyl-vinyl)-benzene, which was a key intermediate to synthesize the various Lamellarins. One method is by using the Wittig-Horner reaction and another is by the Grignard reaction. By conducting contrast experiments, we got the optimal reaction parameters for high yields. The newly formed intermediate was identified by means of IR spectrum, H-1-NMR, C-13-NMR and melting point measurements.
语种: 英语
WOS记录号: WOS:000249597500009
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/140536
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Dalian Univ, Liaoning Key Lab Bioorgan Chem, Dalian 116622, Peoples R China
2.Dalian Univ, Coll Environm & Chem Technol, Dalian 116622, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China

Recommended Citation:
He, Yu-Rong,You, Ye-Cheng,Hu, Jie-Han,et al. Synthesis of a new intermediate for bioactive Lamellarins[J]. BIOMEDICAL MATERIALS,2007,2(2):102-106.
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