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The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography
Dong, Xiaoli1,2; Wu, Ren'an1; Dong, Jing1; Wu, Minghuo1; Zhu, Yan2; Zou, Hanfa1
KeywordCapillary Electrochromatography Covalently Bonded Chiral Stationary Phase Cellulose Tris(3 Enantioseparation 5-dimethylphenylcarbamate) Silica Monolithic Column
Source PublicationJOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES
2008-11-01
DOI10.1016/j.jchromb.2008.05.019
Volume875Issue:1Pages:317-322
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Life Sciences & Biomedicine ; Physical Sciences
WOS SubjectBiochemical Research Methods ; Chemistry, Analytical
WOS Research AreaBiochemistry & Molecular Biology ; Chemistry
WOS KeywordCHIRAL STATIONARY-PHASE ; LIQUID-CHROMATOGRAPHIC ENANTIOSEPARATIONS ; CHARGED POLYACRYLAMIDE-GELS ; ENANTIOMERIC SEPARATIONS ; POLYSACCHARIDE DERIVATIVES ; VANCOMYCIN ; TRIS(3,5-DICHLOROPHENYLCARBAMATE) ; SIZE
AbstractA chiral capillary monolithic column for capillary electrochromatography (CEC) was prepared by covalent bonding of cellulose tris(3,5-dimethylphenylcarbamate) (CDMPC) on the silica monolithic matrix within the confine of a 50-mu m i.d. bare fused silica capillary. Several pairs of enantiomers including neutral and basic analytes were baseline resolved on the newly prepared chiral capillary monolithic column in CEC with aqueous mobile phases. Fast enantioseparation was achieved due to the favorable dynamic properties of silica monolith. The covalent bonding of CDMPC as the chiral stationary phase for CEC also enabled the use of THF in mobile phase for enantioseparation of prazquantel by overcoming the incompatibility of THF and the physically coated CDMPC on a column. (c) 2008 Published by Elsevier B.V.
Language英语
WOS IDWOS:000260945800042
Citation statistics
Cited Times:26[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/140808
Collection中国科学院大连化学物理研究所
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatograph R&A Ctr, Dalian 116023, Peoples R China
2.Zhejiang Univ, Dept Chem, Hangzhou 310028, Peoples R China
Recommended Citation
GB/T 7714
Dong, Xiaoli,Wu, Ren'an,Dong, Jing,et al. The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography[J]. JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES,2008,875(1):317-322.
APA Dong, Xiaoli,Wu, Ren'an,Dong, Jing,Wu, Minghuo,Zhu, Yan,&Zou, Hanfa.(2008).The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography.JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES,875(1),317-322.
MLA Dong, Xiaoli,et al."The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography".JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES 875.1(2008):317-322.
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