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The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography
Dong, Xiaoli1,2; Wu, Ren'an1; Dong, Jing1; Wu, Minghuo1; Zhu, Yan2; Zou, Hanfa1
关键词Capillary Electrochromatography Covalently Bonded Chiral Stationary Phase Cellulose Tris(3 Enantioseparation 5-dimethylphenylcarbamate) Silica Monolithic Column
刊名JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES
2008-11-01
DOI10.1016/j.jchromb.2008.05.019
875期:1页:317-322
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]CHIRAL STATIONARY-PHASE ; LIQUID-CHROMATOGRAPHIC ENANTIOSEPARATIONS ; CHARGED POLYACRYLAMIDE-GELS ; ENANTIOMERIC SEPARATIONS ; POLYSACCHARIDE DERIVATIVES ; VANCOMYCIN ; TRIS(3,5-DICHLOROPHENYLCARBAMATE) ; SIZE
英文摘要A chiral capillary monolithic column for capillary electrochromatography (CEC) was prepared by covalent bonding of cellulose tris(3,5-dimethylphenylcarbamate) (CDMPC) on the silica monolithic matrix within the confine of a 50-mu m i.d. bare fused silica capillary. Several pairs of enantiomers including neutral and basic analytes were baseline resolved on the newly prepared chiral capillary monolithic column in CEC with aqueous mobile phases. Fast enantioseparation was achieved due to the favorable dynamic properties of silica monolith. The covalent bonding of CDMPC as the chiral stationary phase for CEC also enabled the use of THF in mobile phase for enantioseparation of prazquantel by overcoming the incompatibility of THF and the physically coated CDMPC on a column. (c) 2008 Published by Elsevier B.V.
语种英语
WOS记录号WOS:000260945800042
引用统计
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/140808
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatograph R&A Ctr, Dalian 116023, Peoples R China
2.Zhejiang Univ, Dept Chem, Hangzhou 310028, Peoples R China
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GB/T 7714
Dong, Xiaoli,Wu, Ren'an,Dong, Jing,et al. The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography[J]. JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES,2008,875(1):317-322.
APA Dong, Xiaoli,Wu, Ren'an,Dong, Jing,Wu, Minghuo,Zhu, Yan,&Zou, Hanfa.(2008).The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography.JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES,875(1),317-322.
MLA Dong, Xiaoli,et al."The covalently bonded cellulose tris(3,5-dimethylphenylcarbamate) on a silica monolithic capillary column for enantioseparation in capillary electrochromatography".JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES 875.1(2008):317-322.
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