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题名: Preparation of novel beta-cyclodextrin chiral stationary phase based on click chemistry
作者: Zhang, Yongping1;  Guo, Zhimou3;  Ye, Jinxing1;  Xu, Qing3;  Liang, Xinmiao1, 3;  Lei, Aiwen2
关键词: beta-cyclodextrin ;  chiral stationary phases ;  click chemistry ;  chiral separation
刊名: JOURNAL OF CHROMATOGRAPHY A
发表日期: 2008-05-16
DOI: 10.1016/j.chroma.2007.11.018
卷: 1191, 期:1-2, 页:188-192
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Life Sciences & Biomedicine ;  Physical Sciences
类目[WOS]: Biochemical Research Methods ;  Chemistry, Analytical
研究领域[WOS]: Biochemistry & Molecular Biology ;  Chemistry
英文摘要: A facile strategy based on click chemistry for preparation of the structurally well-defined native beta-cyclodextrin (beta-CD) based chiral stationary phase (CSP) was proposed. The beta-CD CSP was evaluated by enatioseparation of benzoin, trans-stilbene oxide, Troger's base, bendroflumethiazide, ketoprofen, chlorthalidone, three flavanone compounds and two beta-adrenergic blocking agents under reversed phase high performance liquid chromatography. The chromatographic results demonstrate the chiral separation ability of click beta-CD CSP and illustrate the usefulness of click chemistry in the preparation of beta-CD based CSP. (c) 2007 Elsevier B.V. All rights reserved.
关键词[WOS]: PERFORMANCE LIQUID-CHROMATOGRAPHY ;  BONDED SILICA-GEL ;  RETENTION BEHAVIOR ;  AROMATIC-COMPOUNDS ;  HPLC ;  SEPARATION ;  ENANTIOSEPARATION ;  DERIVATIVES ;  FACILE ;  IMMOBILIZATION
语种: 英语
WOS记录号: WOS:000256326400021
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/140953
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China
2.Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China

Recommended Citation:
Zhang, Yongping,Guo, Zhimou,Ye, Jinxing,et al. Preparation of novel beta-cyclodextrin chiral stationary phase based on click chemistry[J]. JOURNAL OF CHROMATOGRAPHY A,2008,1191(1-2):188-192.
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