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题名: Thermal decomposition kinetics of the synthetic complex Pb(1,4-BDC)center dot(DMF)(H2O)
作者: Zhang, J.1, 2;  Zeng, J. L.1, 2;  Liu, Y. Y.1;  Sun, L. X.1, 2;  Xu, F.;  You, W. S.3;  Sawada, Y.4
关键词: apparent activation energy ;  kinetic model ;  TG-DTG ;  thermal decomposition
刊名: JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
发表日期: 2008
DOI: 10.1007/s10973-007-8494-9
卷: 91, 期:1, 页:189-193
收录类别: SCI ;  ISTP
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical ;  Chemistry, Physical
研究领域[WOS]: Chemistry
英文摘要: Pb(1,4-BDC)center dot(DMF)(H2O) (1,4-BDC=1,4-benzenedicarboxylate; DMF=dimethylformamide) has been synthesized and investigated by elemental analysis, FTIR spectroscopy, thermogravimetry (TG), derivative thermogravimetry (DTG). TG-DTG curves show that the thermal decomposition occurs in four stages and the corresponding apparent activation energies were calculated with the Ozawa-Flynn-Wall (OFW) and the Friedman methods. The most probable kinetic model function of the dehydration reaction of the compound has been estimated by the Coats-Redfern integral and the Achar-Bridly-Sharp differential methods in this study.
关键词[WOS]: METAL-ORGANIC FRAMEWORK ;  THERMOGRAVIMETRIC DATA ;  COORDINATION POLYMERS ;  DESIGN
语种: 英语
WOS记录号: WOS:000252889200028
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/141027
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
3.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China
4.Tokyo Polytech Univ, Fac Engn, Dept Nanochem, Atsugi, Kanagawa 2430297, Japan

Recommended Citation:
Zhang, J.,Zeng, J. L.,Liu, Y. Y.,et al. Thermal decomposition kinetics of the synthetic complex Pb(1,4-BDC)center dot(DMF)(H2O)[J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY,2008,91(1):189-193.
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