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Fe2O3/SBA-15 catalyst synthesized by chemical vapor infiltration for Friedel-Crafts alkylation reaction
Lei, Zhibin1; Bai, Shiying1; Dang, Liqin1; Xia, Haian2; Xu, Qian2; Cao, Yindi1; An, Lizhen1; Zhao, Mingyi1; Lo, An-Ya3; Liu, Shang-Bin3
KeywordFe2o3/sba-15 Alkylation Reaction Fe/carbon Chemical Vapor Infiltration Mesoporous Carbon
Source PublicationMICROPOROUS AND MESOPOROUS MATERIALS
2009-07-01
DOI10.1016/j.micromeso.2009.04.014
Volume123Issue:1-3Pages:306-313
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences ; Technology
WOS SubjectChemistry, Applied ; Chemistry, Physical ; Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
WOS Research AreaChemistry ; Science & Technology - Other Topics ; Materials Science
WOS KeywordCONTAINING MESOPOROUS MATERIALS ; CARBON MOLECULAR-SIEVES ; BENZYL-CHLORIDE ; IRON-OXIDE ; NANOPOROUS CARBON ; PORE VOLUME ; NANOPARTICLES ; NANOTUBES ; SILICA ; OXIDATION
AbstractFe/SBA-15/carbon composites were synthesized by chemical vapor infiltration (CVI) method using ferrocene as concurrent iron and carbon precursor. Accordingly, Fe2O3 nanoparticles supported on mesoporous SBA-15 silica or metallic Fe homogeneously embedded in mesoporous carbon were selectively obtained either by oxidizing the carbon component in air or by removing the silica template using an aqueous NaOH solution. The Fe2O3/SBA-15 and Fe/carbon composites so obtained were thoroughly characterized by N-2 adsorption/desorption isotherm measurements, powder X-ray diffraction (XRD), transmission electron microscopy and H-2-temperature programmed reduction (H-2-TPR). The effects of CVI duration time and temperature on their corresponding reduction states and particle dispersion, and consequently on their catalytic performances during benzylation reaction of benzene with benzyl chloride were examined and discussed. (C) 2009 Elsevier Inc. All rights reserved.
Language英语
WOS IDWOS:000267099000038
Citation statistics
Cited Times:20[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/141310
Collection中国科学院大连化学物理研究所
Affiliation1.Liaoning Normal Univ, Fac Chem & Chem Engn, Inst Chem Functionalized Mat, Dalian 116029, Liaoning, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
3.Acad Sinica, Inst Atom & Mol Sci, Taipei 10617, Taiwan
Recommended Citation
GB/T 7714
Lei, Zhibin,Bai, Shiying,Dang, Liqin,et al. Fe2O3/SBA-15 catalyst synthesized by chemical vapor infiltration for Friedel-Crafts alkylation reaction[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2009,123(1-3):306-313.
APA Lei, Zhibin.,Bai, Shiying.,Dang, Liqin.,Xia, Haian.,Xu, Qian.,...&Liu, Shang-Bin.(2009).Fe2O3/SBA-15 catalyst synthesized by chemical vapor infiltration for Friedel-Crafts alkylation reaction.MICROPOROUS AND MESOPOROUS MATERIALS,123(1-3),306-313.
MLA Lei, Zhibin,et al."Fe2O3/SBA-15 catalyst synthesized by chemical vapor infiltration for Friedel-Crafts alkylation reaction".MICROPOROUS AND MESOPOROUS MATERIALS 123.1-3(2009):306-313.
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