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Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry
Ding, Li1; Xie, Fuwei1; Xu, Guowang2; Liu, Kejian1; Wang, Sheng1; Xie, Jianping1
KeywordEsi/ms Normal-phase Lc Rplc Tobacco Cuticular Components
Source PublicationJOURNAL OF SEPARATION SCIENCE
2010-11-01
DOI10.1002/jssc.201000536
Volume33Issue:21Pages:3429-3436
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences
WOS SubjectChemistry, Analytical
WOS Research AreaChemistry
WOS Keyword2-DIMENSIONAL GAS-CHROMATOGRAPHY ; TRADITIONAL CHINESE MEDICINES ; SUCROSE ESTERS ; ION-EXCHANGE ; MACROCYCLIC DITERPENES ; LABDANIC COMPOUNDS ; GREEK TOBACCO ; CHEMISTRY ; VOLATILE ; CEMBRATRIENETRIOLS
AbstractIntegration of normal-phase LC (NPLC) fractionation with RPLC-ESI/MS was established to detect the polar fractions of cuticular components from Oriental tobacco leaf. NPLC was selected for the fractionation of polar components of cuticular leaf extract, after being concentrated with rotary evaporator, each of the enriched fractions was further analyzed by RPLC-ESI/MS. In total, 83 compounds were finally detected including 45 cembranoids, 15 labdanoids, 20 sucrose esters, and 3 glucose esters (or fructose esters). Three cembranoids and seven labdanoids possibly are new diterpenoids. Glucose esters (or fructose esters) are also reported in Nicotiana tobacco for the first time.
Language英语
WOS IDWOS:000284230700020
Citation statistics
Cited Times:6[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/141673
Collection中国科学院大连化学物理研究所
Affiliation1.Zhengzhou Tobacco Res Inst CNTC, Key Lab Tobacco Chem, Zhengzhou 450001, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, CAS Key Lab Separat Sci Analyt Chem, Dalian, Peoples R China
Recommended Citation
GB/T 7714
Ding, Li,Xie, Fuwei,Xu, Guowang,et al. Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry[J]. JOURNAL OF SEPARATION SCIENCE,2010,33(21):3429-3436.
APA Ding, Li,Xie, Fuwei,Xu, Guowang,Liu, Kejian,Wang, Sheng,&Xie, Jianping.(2010).Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry.JOURNAL OF SEPARATION SCIENCE,33(21),3429-3436.
MLA Ding, Li,et al."Separation and detection of polar cuticular components from Oriental tobacco leaf by integration of normal-phase liquid chromatography fractionation with reversed-phase liquid chromatography-mass spectrometry".JOURNAL OF SEPARATION SCIENCE 33.21(2010):3429-3436.
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