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Chemically bonded maltose via click chemistry as stationary phase for HILIC
Fu, Qing1; Guo, Zhimou1; Liang, Tu2; Zhang, Xiuli1; Xu, Qing1; Liang, Xinmiao1,2
刊名ANALYTICAL METHODS
2010-03-01
DOI10.1039/b9ay00151d
2期:3页:217-224
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences ; Life Sciences & Biomedicine ; Technology
类目[WOS]Chemistry, Analytical ; Food Science & Technology ; Spectroscopy
研究领域[WOS]Chemistry ; Food Science & Technology ; Spectroscopy
关键词[WOS]HYDROPHILIC-INTERACTION CHROMATOGRAPHY ; INTERACTION LIQUID-CHROMATOGRAPHY ; SELF-ASSEMBLED MONOLAYERS ; SMALL POLAR COMPOUNDS ; MASS-SPECTROMETRY ; REVERSED-PHASE ; BETA-CYCLODEXTRIN ; AFFINITY-CHROMATOGRAPHY ; EXCHANGE CHROMATOGRAPHY ; MOBILE-PHASE
英文摘要A HILIC stationary phase was synthesized through bonding maltose on silica particles via click chemistry A set of representative polar compounds including sugars, ammo acids and small peptides were employed to evaluate chromatographic properties of Click Maltose The results illustrated the surface adsorption mechanism from the direct hydrogen bonding interaction between sugars and Click Maltose played an important role on retention behavior of sugars under HILIC mode The chromatographic behavior of anions on Click Maltose was consistent with HILIC/WAX mechanism, while the retention of cations was depended on electrostatic repulsion-hydrophilic interaction chromatography (ERLIC) mechanism The Click Maltose stationary phase was successfully used in the separation of standard samples of polar compounds and complex samples of oligosaccharides from the natural product The Click Maltose also exhibited good reproducibility and stability, which were helpful to further application Our study confirmed the advantages and application potential of bonded oligosaccharides for HILIC separation
语种英语
WOS记录号WOS:000276805900003
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被引频次:41[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/141717
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Grad Sch, Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China
2.E China Univ Sci & Technol, Sch Pharm, Minist Educ, Engn Res Ctr Pharmaceut Proc Chem, Shanghai 200237, Peoples R China
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GB/T 7714
Fu, Qing,Guo, Zhimou,Liang, Tu,et al. Chemically bonded maltose via click chemistry as stationary phase for HILIC[J]. ANALYTICAL METHODS,2010,2(3):217-224.
APA Fu, Qing,Guo, Zhimou,Liang, Tu,Zhang, Xiuli,Xu, Qing,&Liang, Xinmiao.(2010).Chemically bonded maltose via click chemistry as stationary phase for HILIC.ANALYTICAL METHODS,2(3),217-224.
MLA Fu, Qing,et al."Chemically bonded maltose via click chemistry as stationary phase for HILIC".ANALYTICAL METHODS 2.3(2010):217-224.
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