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Cooperative structure-directing effect in the synthesis of aluminophosphate molecular sieves in ionic liquids
Xu, Renshun1; Shi, Xiaochao2; Zhang, Weiping1; Xu, Yunpeng1; Tian, Zhijian1; Lu, Xiaobing2; Han, Xiuwen1; Bao, Xinhe1
刊名PHYSICAL CHEMISTRY CHEMICAL PHYSICS
2010
DOI10.1039/b920232n
12期:10页:2443-2449
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Physical ; Physics, Atomic, Molecular & Chemical
研究领域[WOS]Chemistry ; Physics
关键词[WOS]IONOTHERMAL SYNTHESIS ; FLUORESCENCE BEHAVIOR ; ZEOLITE ; NMR ; CRYSTALLIZATION ; TEMPLATE ; AGENTS ; DERIVATIVES ; FRAMEWORKS ; CHEMISTRY
英文摘要In situ two-dimensional NMR and fluorescence emission spectroscopy were employed to investigate the cooperative structure-direction effect of organic amine such as morpholine in the synthesis of aluminophosphate molecular sieves in ionic liquids. In situ rotating frame nuclear Overhauser effect spectra (ROESY) together with fluorescence measurements demonstrate that the aggregates between imidazolium cations and morpholines through intermolecular hydrogen bonds can be formed in the gel during the crystallization of molecular sieves. Combining with the characterizations of the solid products by solid-state NMR, it is verified that different aggregates of organic amines with imidazolium cations, which is similar to self-assembled supramolecular analogues, could act as the structure-directing agents for selective tuning of the framework topologies such as AEL, AFI and LTA in the final solid products.
语种英语
WOS记录号WOS:000274920200020
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/141741
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
2.Dalian Univ Technol, State Key Lab Fine Chem, Dalian 116012, Peoples R China
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Xu, Renshun,Shi, Xiaochao,Zhang, Weiping,et al. Cooperative structure-directing effect in the synthesis of aluminophosphate molecular sieves in ionic liquids[J]. PHYSICAL CHEMISTRY CHEMICAL PHYSICS,2010,12(10):2443-2449.
APA Xu, Renshun.,Shi, Xiaochao.,Zhang, Weiping.,Xu, Yunpeng.,Tian, Zhijian.,...&Bao, Xinhe.(2010).Cooperative structure-directing effect in the synthesis of aluminophosphate molecular sieves in ionic liquids.PHYSICAL CHEMISTRY CHEMICAL PHYSICS,12(10),2443-2449.
MLA Xu, Renshun,et al."Cooperative structure-directing effect in the synthesis of aluminophosphate molecular sieves in ionic liquids".PHYSICAL CHEMISTRY CHEMICAL PHYSICS 12.10(2010):2443-2449.
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