DICP OpenIR
Isolation of inulin-type oligosaccharides from Chinese traditional medicine: Morinda officinalis How and their characterization using ESI-MS/MS
Yang, Zhenmin1,2; Yi, Yongtao1; Gao, Chuanchuan1; Hou, Dengke3; Hu, Jun1; Zhao, Mingyue1
关键词Characterization Esi-ms Inulin-type Oligosaccharide Isolation Morinda Officinalis How
刊名JOURNAL OF SEPARATION SCIENCE
2010
DOI10.1002/jssc.200900396
33期:1页:120-125
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]CYCLODEXTRIN-BONDED PHASE ; MASS-SPECTROMETRY ; ELECTROSPRAY-IONIZATION ; UNDERIVATIZED OLIGOSACCHARIDES ; XYLO-OLIGOSACCHARIDES ; LIQUID-CHROMATOGRAPHY ; PC12 CELLS ; SEPARATION ; CORTICOSTERONE ; CREAM
英文摘要Inulin-type oligosaccharides with different DP were prepared by size-exclusion chromatography and purity of each oligosaccharide was determined by HPLC equipped with cyclodextrin-bond column. The purities of obtained inulin-type oligosaccharides with different DP were more than 98% by one-step process. The DP and molecular weight were obtained through ESI-MS in negative mode. The characterization of the inulin-type oligosaccharides with different DP was studied by MS/MS spectra obtained by collision-induced dissociation of molecular ions ([M-H](-)). When the DP was lower, the fragment ions were formed through cross-ring cleavages of two bonds within the sugar ring and glycosidic cleavages. However, with the increase of DP, the ions resulting from glycosidic cleavages between two sugar residues were predominant.
语种英语
WOS记录号WOS:000274306800015
引用统计
被引频次:24[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/141778
专题中国科学院大连化学物理研究所
作者单位1.Zhengzhou Tobacco Res Inst CNTC, Lab Flavor & Fragrance, Zhengzhou 450001, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Key Lab Separat Sci Analyt Chem, Dalian, Peoples R China
3.Zhengzhou Univ, Dept Chem, Zhengzhou 450052, Peoples R China
推荐引用方式
GB/T 7714
Yang, Zhenmin,Yi, Yongtao,Gao, Chuanchuan,et al. Isolation of inulin-type oligosaccharides from Chinese traditional medicine: Morinda officinalis How and their characterization using ESI-MS/MS[J]. JOURNAL OF SEPARATION SCIENCE,2010,33(1):120-125.
APA Yang, Zhenmin,Yi, Yongtao,Gao, Chuanchuan,Hou, Dengke,Hu, Jun,&Zhao, Mingyue.(2010).Isolation of inulin-type oligosaccharides from Chinese traditional medicine: Morinda officinalis How and their characterization using ESI-MS/MS.JOURNAL OF SEPARATION SCIENCE,33(1),120-125.
MLA Yang, Zhenmin,et al."Isolation of inulin-type oligosaccharides from Chinese traditional medicine: Morinda officinalis How and their characterization using ESI-MS/MS".JOURNAL OF SEPARATION SCIENCE 33.1(2010):120-125.
条目包含的文件
条目无相关文件。
个性服务
推荐该条目
保存到收藏夹
查看访问统计
导出为Endnote文件
谷歌学术
谷歌学术中相似的文章
[Yang, Zhenmin]的文章
[Yi, Yongtao]的文章
[Gao, Chuanchuan]的文章
百度学术
百度学术中相似的文章
[Yang, Zhenmin]的文章
[Yi, Yongtao]的文章
[Gao, Chuanchuan]的文章
必应学术
必应学术中相似的文章
[Yang, Zhenmin]的文章
[Yi, Yongtao]的文章
[Gao, Chuanchuan]的文章
相关权益政策
暂无数据
收藏/分享
所有评论 (0)
暂无评论
 

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。