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题名: Low-Temperature Synthesis and Characterization of AlPO-Cristobalite in Ionic Liquid
作者: Xu Renshun1;  Zhang Weiping1;  Han Xiuwen1;  Bao Xinhe1
关键词: ionothermal synthesis ;  aluminophosphate ;  cristobalite ;  solid state nuclear magnetic resonance ;  ionic liquid
刊名: CHINESE JOURNAL OF CATALYSIS
发表日期: 2010-07-01
DOI: 10.3724/SP.J.1088.2010.91139
卷: 31, 期:7, 页:776-780
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences ;  Technology
类目[WOS]: Chemistry, Applied ;  Chemistry, Physical ;  Engineering, Chemical
研究领域[WOS]: Chemistry ;  Engineering
英文摘要: AlPO-cristobalite was prepared at low temperature of 80 degrees C for 30 min in the [bmim]Br ionic liquid. The effects of reaction conditions, such as the amount of organic amine and HF acid, the P/Al ratio, and reaction time, were investigated in detail in the ionothermal synthesis. Powder X-ray diffraction and high-resolution solid-state NMR show that the resultant sample is alpha-AlPO-cristobalite, and most of the Al and P species are located on the framework and connected by Al-O-P tetrahedron.
关键词[WOS]: SOLID-STATE NMR ;  IONOTHERMAL SYNTHESIS ;  MOLECULAR-SIEVES ;  PHOSPHATE ;  NANOPARTICLES ;  ZEOLITES ;  TEMPLATE ;  AMINES
语种: 英语
WOS记录号: WOS:000280868900010
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/141816
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Liaoning, Peoples R China

Recommended Citation:
Xu Renshun,Zhang Weiping,Han Xiuwen,et al. Low-Temperature Synthesis and Characterization of AlPO-Cristobalite in Ionic Liquid[J]. CHINESE JOURNAL OF CATALYSIS,2010,31(7):776-780.
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