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Ionothermal synthesis and crystal structure of a new layered nickel(II) diphosphate, DRM-1
Wei, Ying1,2; Gies, Hermann3; Tian, Zhijian1; Marler, Bernd3; Xu, Yunpeng1; Wang, Lei1; Ma, Huaijun1; Pei, Renyan1,2; Li, Keda1,2; Wang, Bingchun1
关键词Ionothermal Synthesis Ionic Liquids Nickel Diphosphate Open-framework Layered Structure
刊名INORGANIC CHEMISTRY COMMUNICATIONS
2010-11-01
DOI10.1016/j.inoche.2010.07.036
13期:11页:1357-1360
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Inorganic & Nuclear
研究领域[WOS]Chemistry
关键词[WOS]MAGNETIC-PROPERTIES ; SPECTROSCOPIC PROPERTIES ; HYDROTHERMAL SYNTHESIS ; PHOSPHATE VSB-5 ; ALUMINOPHOSPHATE ; BEHAVIOR ; FRAMEWORKS ; CATALYST
英文摘要A new layered ammonium nickel(II) diphosphate, (NH(4))(2)[Ni(3)(P(2)O(7))(2)(H(2)O)(2)], has been synthesized ionothermally in the ionic liquid 1-butyl-3-methyl imidazolium bromide and characterized by powder X-ray diffraction, elemental analysis, scaning electron microscopy, thermogravimetry etc. The results of the characterization show that the crystal adopts the monoclinic space group P2(1)/a with the lattice constants a=9.23529(2) angstrom, b=7.98489(2) angstrom. c=9.40772(2) angstrom, beta=100.2608(2)degrees and Z=2. Its structure consists of chains of cis- and trans-edge-sharing [NiO(6)](-)octahedra linked via [P(2)O(7)] units to form layers of [Ni(3)(P(2)O(7))(2) (H(2)O)(2)](2-) in the ab plane. Adjacent layers are separated in the c-direction by ammonium ions. (C) 2010 Elsevier B.V. All rights reserved.
语种英语
WOS记录号WOS:000282867800034
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/142090
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian Natl Lab Clean Energy, State Key Lab Catalysis, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China
3.Ruhr Univ Bochum, Inst Geol Mineral & Geophys, D-44780 Bochum, Germany
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Wei, Ying,Gies, Hermann,Tian, Zhijian,et al. Ionothermal synthesis and crystal structure of a new layered nickel(II) diphosphate, DRM-1[J]. INORGANIC CHEMISTRY COMMUNICATIONS,2010,13(11):1357-1360.
APA Wei, Ying.,Gies, Hermann.,Tian, Zhijian.,Marler, Bernd.,Xu, Yunpeng.,...&Wang, Bingchun.(2010).Ionothermal synthesis and crystal structure of a new layered nickel(II) diphosphate, DRM-1.INORGANIC CHEMISTRY COMMUNICATIONS,13(11),1357-1360.
MLA Wei, Ying,et al."Ionothermal synthesis and crystal structure of a new layered nickel(II) diphosphate, DRM-1".INORGANIC CHEMISTRY COMMUNICATIONS 13.11(2010):1357-1360.
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