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题名: Ionothermal synthesis and crystal structure of a new layered nickel(II) diphosphate, DRM-1
作者: Wei, Ying1, 2;  Gies, Hermann3;  Tian, Zhijian1;  Marler, Bernd3;  Xu, Yunpeng1;  Wang, Lei1;  Ma, Huaijun1;  Pei, Renyan1, 2;  Li, Keda1, 2;  Wang, Bingchun1
关键词: Ionothermal synthesis ;  Ionic liquids ;  Nickel diphosphate ;  Open-framework ;  Layered structure
刊名: INORGANIC CHEMISTRY COMMUNICATIONS
发表日期: 2010-11-01
DOI: 10.1016/j.inoche.2010.07.036
卷: 13, 期:11, 页:1357-1360
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Inorganic & Nuclear
研究领域[WOS]: Chemistry
英文摘要: A new layered ammonium nickel(II) diphosphate, (NH(4))(2)[Ni(3)(P(2)O(7))(2)(H(2)O)(2)], has been synthesized ionothermally in the ionic liquid 1-butyl-3-methyl imidazolium bromide and characterized by powder X-ray diffraction, elemental analysis, scaning electron microscopy, thermogravimetry etc. The results of the characterization show that the crystal adopts the monoclinic space group P2(1)/a with the lattice constants a=9.23529(2) angstrom, b=7.98489(2) angstrom. c=9.40772(2) angstrom, beta=100.2608(2)degrees and Z=2. Its structure consists of chains of cis- and trans-edge-sharing [NiO(6)](-)octahedra linked via [P(2)O(7)] units to form layers of [Ni(3)(P(2)O(7))(2) (H(2)O)(2)](2-) in the ab plane. Adjacent layers are separated in the c-direction by ammonium ions. (C) 2010 Elsevier B.V. All rights reserved.
关键词[WOS]: MAGNETIC-PROPERTIES ;  SPECTROSCOPIC PROPERTIES ;  HYDROTHERMAL SYNTHESIS ;  PHOSPHATE VSB-5 ;  ALUMINOPHOSPHATE ;  BEHAVIOR ;  FRAMEWORKS ;  CATALYST
语种: 英语
WOS记录号: WOS:000282867800034
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/142167
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian Natl Lab Clean Energy, State Key Lab Catalysis, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China
3.Ruhr Univ Bochum, Inst Geol Mineral & Geophys, D-44780 Bochum, Germany

Recommended Citation:
Wei, Ying,Gies, Hermann,Tian, Zhijian,et al. Ionothermal synthesis and crystal structure of a new layered nickel(II) diphosphate, DRM-1[J]. INORGANIC CHEMISTRY COMMUNICATIONS,2010,13(11):1357-1360.
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