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Room temperature ionic liquid-mediated molecularly imprinted polymer monolith for the selective recognition of quinolones in pork samples
Sun, Xiangli2; He, Jia1; Cai, Guorui1; Lin, Anqing1; Zheng, Wenjie1; Liu, Xuan1; Chen, Langxing2; He, Xiwen2; Zhang, Yukui2,3
关键词Molecularly Imprinted Polymer Monolith Pork Samples Quinolone Antibiotics Room Temperature Ionic Liquids Selective Recognition
刊名JOURNAL OF SEPARATION SCIENCE
2010-12-01
DOI10.1002/jssc.201000337
33期:23-24页:3786-3793
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]SOLID-PHASE EXTRACTION ; CAPILLARY ELECTROCHROMATOGRAPHY ; CHROMATOGRAPHY ; FLUOROQUINOLONES ; CIPROFLOXACIN ; TISSUE ; COLUMN ; URINE
英文摘要A novel molecularly imprinted polymer monolith was prepared by the room temperature ionic liquid-mediated in situ molecular imprinting technique, using norfloxacin (NOR) as the template, methacrylic acid as the functional monomer, ethylene glycol dimethacrylate as the cross-linker. The optimal synthesis conditions and recognition properties of NOR-imprinted monolithic column were investigated. The results indicated that the imprinted monoliths exhibited good ability of selective recognition against the template and its structural analog. Using the fabricated material as solid-phase extraction sorbent, a sample pre-treatment procedure of molecularly imprinted solid-phase extraction coupling with HPLC was developed for determination of trace quinolone residues in animal tissues samples. The recoveries ranging from 78.16 to 93.50% for eight quinolones antibiotics such as marbofloxacin, NOR, ciprofloxacin, danofloxacin, difloxacin, oxolinic acid, flumequine and enrofloxacin were obtained.
语种英语
WOS记录号WOS:000285312700022
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被引频次:44[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/142233
专题中国科学院大连化学物理研究所
作者单位1.Tianjin Entry Exit Inspect & Quarantine Bur, Anim Plant & Food Inspect Ctr, Tianjin, Peoples R China
2.Nankai Univ, Dept Chem, Tianjin 300071, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian, Peoples R China
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Sun, Xiangli,He, Jia,Cai, Guorui,et al. Room temperature ionic liquid-mediated molecularly imprinted polymer monolith for the selective recognition of quinolones in pork samples[J]. JOURNAL OF SEPARATION SCIENCE,2010,33(23-24):3786-3793.
APA Sun, Xiangli.,He, Jia.,Cai, Guorui.,Lin, Anqing.,Zheng, Wenjie.,...&Zhang, Yukui.(2010).Room temperature ionic liquid-mediated molecularly imprinted polymer monolith for the selective recognition of quinolones in pork samples.JOURNAL OF SEPARATION SCIENCE,33(23-24),3786-3793.
MLA Sun, Xiangli,et al."Room temperature ionic liquid-mediated molecularly imprinted polymer monolith for the selective recognition of quinolones in pork samples".JOURNAL OF SEPARATION SCIENCE 33.23-24(2010):3786-3793.
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