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学科主题物理化学
Magnetic and Thermodynamic Properties of Nanosized Zn Ferrite with Normal Spinal Structure Synthesized Using a Facile Method
Zhang, Yunong1; Shi, Quan2; Schliesser, Jacob3; Woodfield, Brian F.3; Nan, Zhaodong1; Shi Q(史全); ZhaodongNan
刊名INORGANIC CHEMISTRY
2014-10-06
DOI10.1021/ic501487c
53期:19页:10463-10470
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Inorganic & Nuclear
研究领域[WOS]Chemistry
关键词[WOS]TEMPERATURE HEAT-CAPACITY ; ZINC FERRITE ; GLASS BEHAVIOR ; PARTICLE-SIZE ; NEUTRON-DIFFRACTION ; SURFACE-WATER ; THIN-FILMS ; MFE2O4 M ; ZNFE2O4 ; NANOPARTICLES
英文摘要Normal spinel zinc ferrite (ZnFe2O4) nanoparticles (NPs) with zero net magnetization were synthesized by a facile coprecipitation method in which two kinds of organic alkali, namely, 1-amino-2-propanol (MIPA) and bis(2-hydroxypropyl)-amine (DIPA), were used. The diameters of the ZnFe2O4 NPs were determined to be about 7 and 9 nm for samples prepared with MIPA and DIPA, respectively, and the normal spinel structure was confirmed by the magnetic property measurement at room temperature and the temperature dependence of the direct current magnetization. These results are different from those reported in the literature, where ZnFe2O4 NPs show a nonzero net magnetization. The heat capacity of the ZnFe2O4 NPs synthesized using DIPA was measured using a physical property measurement system in the temperature range from 2 to 300 K, and the thermodynamic functions were calculated based on the curve fitting of the experimental heat capacity data. The heat capacity of the ZnFe2O4 NPs was compared with that of a nanosized (Zn0.795Fe0.205)[Zn0.205Fe1.795]O-4 material studied in the literature, indicating that the Debye temperature of the present sample is more comparable with that of the bulk ZnFe2O4 reported by Westrum et al.
语种英语
WOS记录号WOS:000342856800059
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文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/143882
专题中国科学院大连化学物理研究所
通讯作者Shi Q(史全); ZhaodongNan
作者单位1.Yang Zhou Univ, Coll Chem & Chem Engn, Yangzhou 225002, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Thermochem Lab, Dalian 116023, Liaoning, Peoples R China
3.Brigham Young Univ, Dept Chem & Biochem, Provo, UT 84602 USA
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Zhang, Yunong,Shi, Quan,Schliesser, Jacob,et al. Magnetic and Thermodynamic Properties of Nanosized Zn Ferrite with Normal Spinal Structure Synthesized Using a Facile Method[J]. INORGANIC CHEMISTRY,2014,53(19):10463-10470.
APA Zhang, Yunong.,Shi, Quan.,Schliesser, Jacob.,Woodfield, Brian F..,Nan, Zhaodong.,...&ZhaodongNan.(2014).Magnetic and Thermodynamic Properties of Nanosized Zn Ferrite with Normal Spinal Structure Synthesized Using a Facile Method.INORGANIC CHEMISTRY,53(19),10463-10470.
MLA Zhang, Yunong,et al."Magnetic and Thermodynamic Properties of Nanosized Zn Ferrite with Normal Spinal Structure Synthesized Using a Facile Method".INORGANIC CHEMISTRY 53.19(2014):10463-10470.
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