DICP OpenIR
Rapid Screening of Trace Phthalate Estersin-Wine Using Ion Mobility Spectrometry
Peng Li-Ying1,2; Wang Wei-Guo1; Wang Xin1; Chen Wen-Dong1,2; Chen Chuang1,2; Cheng Sha-Sha1,2; Liang Xi-Xi1,2; Zhou Qing-Hua1,2; Li Jing-Hua1; Li Hai-Yang1
KeywordIon Mobility Spectrometry Phthalate Esters Rapid Screening Plasticizer
Source PublicationCHINESE JOURNAL OF ANALYTICAL CHEMISTRY
2014
Volume42Issue:2Pages:278-282
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences
WOS SubjectChemistry, Analytical
WOS Research AreaChemistry
WOS KeywordPERFORMANCE LIQUID-CHROMATOGRAPHY ; MASS-SPECTROMETRY ; ACID ESTERS
AbstractPhthalic acid ester is a kind of common environmental pollutants. Here, a method for fast screening trace phthalic acid ester in wine was constructed based on ion mobility spectrometry (IMS). Tube temperature and inlet temperature were optimized, and five typical phthalic acid esters were detected successively. Under the optimal tube temperature of 90 degrees C and inlet temperature of 160 degrees C, the limits of detection for dimethyl phthalate (DMP), diethyl phthalate (DEP), dibutyl phthalate (DBP), diisobutyl phthalate (DIBP) and diethylhexyl phthalate (DEHP) are 0.14, 0.06, 0.14, 0.44 and 0.02 mg/L, respectively, and the relative standard deviation (RSD) of 9 times measurements are less than 8.9%. The analytical time for single sample is less than 95 s. At last, five types of white wines were analyzed and the suspicious problem samples were successfully screened. And a home. made ion trap mass spectrometer was used to verify the product ions of phthalic acid ester detected by IMS and the interferences in wines can be avoided with acetone as dopant. The results demonstrate that the IMS can be used for rapid screening of trace phthalate esters in wine.
Language英语
WOS IDWOS:000333673600020
Citation statistics
Cited Times:3[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/145848
Collection中国科学院大连化学物理研究所
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
2.Grad Chinese Acad Sci, Beijing 100039, Peoples R China
Recommended Citation
GB/T 7714
Peng Li-Ying,Wang Wei-Guo,Wang Xin,et al. Rapid Screening of Trace Phthalate Estersin-Wine Using Ion Mobility Spectrometry[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2014,42(2):278-282.
APA Peng Li-Ying.,Wang Wei-Guo.,Wang Xin.,Chen Wen-Dong.,Chen Chuang.,...&Li Hai-Yang.(2014).Rapid Screening of Trace Phthalate Estersin-Wine Using Ion Mobility Spectrometry.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,42(2),278-282.
MLA Peng Li-Ying,et al."Rapid Screening of Trace Phthalate Estersin-Wine Using Ion Mobility Spectrometry".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 42.2(2014):278-282.
Files in This Item:
There are no files associated with this item.
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Peng Li-Ying]'s Articles
[Wang Wei-Guo]'s Articles
[Wang Xin]'s Articles
Baidu academic
Similar articles in Baidu academic
[Peng Li-Ying]'s Articles
[Wang Wei-Guo]'s Articles
[Wang Xin]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Peng Li-Ying]'s Articles
[Wang Wei-Guo]'s Articles
[Wang Xin]'s Articles
Terms of Use
No data!
Social Bookmark/Share
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.